2,3-dihydro-6,7-bis(hydroxymethyl)-5-phenylsulfinyl-1H-pyrrolizine bis-

Base Information

Chemical Name:2,3-dihydro-6,7-bis(hydroxymethyl)-5-phenylsulfinyl-1H-pyrrolizine bis-
CAS No.:129503-36-2
Molecular Formula:C₂₃H₃₁N₃O₅S
Molecular Weight:461.582
Hs Code.:

2,3-dihydro-6,7-bis(hydroxymethyl)-5-phenylsulfinyl-1H-pyrrolizine bis-<N-(2-propyl)carbamate>

Synonyms:2,3-dihydro-6,7-bis(hydroxymethyl)-5-phenylsulfinyl-1H-pyrrolizine bis-

Suppliers and Price of 2,3-dihydro-6,7-bis(hydroxymethyl)-5-phenylsulfinyl-1H-pyrrolizine bis-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2,3-dihydro-6,7-bis(hydroxymethyl)-5-phenylsulfinyl-1H-pyrrolizine bis-

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,3-dihydro-6,7-bis(hydroxymethyl)-5-phenylsulfinyl-1H-pyrrolizine bis-

There total 6 articles about 2,3-dihydro-6,7-bis(hydroxymethyl)-5-phenylsulfinyl-1H-pyrrolizine bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 129524-65-8
2,3-dihydro-6,7-bis(hydroxymethyl)-5-phenylthio-1H-pyrrolizine bis-

: 129503-36-2
2,3-dihydro-6,7-bis(hydroxymethyl)-5-phenylsulfinyl-1H-pyrrolizine bis-

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 0.166667h;
DOI:10.1002/jhet.5570270440

Reference yield:

: 62563-06-8
dimethyl 2,3-dihydro-1H-pyrrolizine-6,7-dicarboxylate

: 129503-36-2
2,3-dihydro-6,7-bis(hydroxymethyl)-5-phenylsulfinyl-1H-pyrrolizine bis-

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / CH₂Cl₂ / 0.25 h / Ambient temperature

2: 62 percent / LiAlH₄ / tetrahydrofuran / 2 h / Ambient temperature

3: 41 percent / m-chloroperoxbenzoic acid / CH₂Cl₂ / 0.17 h / 0 °C

With lithium aluminium tetrahydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1002/jhet.5570270440

Reference yield:

: 500889-75-8
6,7-bis(hydroxymethyl)-2,3-dihydro-1H-pyrrolizine

: 129503-36-2
2,3-dihydro-6,7-bis(hydroxymethyl)-5-phenylsulfinyl-1H-pyrrolizine bis-

Guidance literature:: Multi-step reaction with 3 steps

1: di-n-butyltin diacetate

2: 78 percent / triethylamine / CH₂Cl₂ / 0.17 h / Ambient temperature

3: 41 percent / m-chloroperoxbenzoic acid / CH₂Cl₂ / 0.17 h / 0 °C

With dibutyltin diacetate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1002/jhet.5570270440