6-Carbomethoxymethyl-3,4-dimethoxybenzenesulfonyl chloride

Base Information

Chemical Name:6-Carbomethoxymethyl-3,4-dimethoxybenzenesulfonyl chloride
CAS No.:62208-38-2
Molecular Formula:C₁₁H₁₃ClO₆S
Molecular Weight:308.74
Hs Code.:

Synonyms:6-Carbomethoxymethyl-3,4-dimethoxybenzenesulfonyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-Carbomethoxymethyl-3,4-dimethoxybenzenesulfonyl chloride

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Technology Process of 6-Carbomethoxymethyl-3,4-dimethoxybenzenesulfonyl chloride

There total 3 articles about 6-Carbomethoxymethyl-3,4-dimethoxybenzenesulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 15964-79-1
methyl (3,4-dimethoxyphenyl)acetate

: 62208-38-2
6-Carbomethoxymethyl-3,4-dimethoxybenzenesulfonyl chloride

Guidance literature:: With chlorosulfonic acid; In chloroform; at 0 - 20 ℃; for 4h; Inert atmosphere;

Reference yield:

: 93-40-3
(3,4-Dimethoxyphenyl)acetic acid

: 62208-38-2
6-Carbomethoxymethyl-3,4-dimethoxybenzenesulfonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere

1.2: 0.17 h / 0 - 20 °C / Inert atmosphere

2.1: chlorosulfonic acid / chloroform / 1 h / 0 - 20 °C / Inert atmosphere

With chlorosulfonic acid; oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; chloroform;
DOI:10.2147/OTT.S254856