benzyl 5-(acetoxymethyl)-4-<(ethoxycarbonyl)methyl>-3-<2-(methoxycarbonyl)ethyl>pyrrole-2-carboxylate

Base Information

Chemical Name:benzyl 5-(acetoxymethyl)-4-<(ethoxycarbonyl)methyl>-3-<2-(methoxycarbonyl)ethyl>pyrrole-2-carboxylate
CAS No.:220720-50-3
Molecular Formula:C₂₃H₂₇NO₈
Molecular Weight:445.469
Hs Code.:

Synonyms:benzyl 5-(acetoxymethyl)-4-<(ethoxycarbonyl)methyl>-3-<2-(methoxycarbonyl)ethyl>pyrrole-2-carboxylate

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Chemical Property of benzyl 5-(acetoxymethyl)-4-<(ethoxycarbonyl)methyl>-3-<2-(methoxycarbonyl)ethyl>pyrrole-2-carboxylate

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Technology Process of benzyl 5-(acetoxymethyl)-4-<(ethoxycarbonyl)methyl>-3-<2-(methoxycarbonyl)ethyl>pyrrole-2-carboxylate

There total 3 articles about benzyl 5-(acetoxymethyl)-4-<(ethoxycarbonyl)methyl>-3-<2-(methoxycarbonyl)ethyl>pyrrole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 108-24-7
acetic anhydride

: 220720-48-9
benzyl 4-<(ethoxycarbonyl)methyl>-3-<2-(methoxycarbonyl)ethyl>-5-methylpyrrole-2-carboxylate

: 220720-50-3
benzyl 5-(acetoxymethyl)-4-<(ethoxycarbonyl)methyl>-3-<2-(methoxycarbonyl)ethyl>pyrrole-2-carboxylate

Guidance literature:: With lead(IV) acetate; In acetic acid; for 2h; Ambient temperature;
DOI:10.1021/jo9814748

Reference yield:

: 80480-42-8
methyl 4,6-dioxoheptanoate, keto-tautomer

: 220720-50-3
benzyl 5-(acetoxymethyl)-4-<(ethoxycarbonyl)methyl>-3-<2-(methoxycarbonyl)ethyl>pyrrole-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 40 percent / potassium carbonate / acetone / 5 h / Heating

2: 39 percent / zinc dust, sodium acetate / acetic acid / 1 h / 90 °C

3: 94 percent / lead tetraacetate / acetic acid / 2 h / Ambient temperature

With lead(IV) acetate; sodium acetate; potassium carbonate; zinc; In acetic acid; acetone;
DOI:10.1021/jo9814748

Reference yield:

: 220720-49-0
methyl 5-<(ethoxycarbonyl)methyl>-4,6-dioxoheptanoate

: 220720-50-3
benzyl 5-(acetoxymethyl)-4-<(ethoxycarbonyl)methyl>-3-<2-(methoxycarbonyl)ethyl>pyrrole-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 39 percent / zinc dust, sodium acetate / acetic acid / 1 h / 90 °C

2: 94 percent / lead tetraacetate / acetic acid / 2 h / Ambient temperature

With lead(IV) acetate; sodium acetate; zinc; In acetic acid;
DOI:10.1021/jo9814748