Technology Process of 4-amino-α-(6,7-dimethoxy-1-isoquinolinyl)-m-cresol
There total 4 articles about 4-amino-α-(6,7-dimethoxy-1-isoquinolinyl)-m-cresol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen; potassium carbonate;
palladium on activated charcoal;
In
ethanol;
for 3h;
under 2947.7 Torr;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) benzyltrimethylammonium chloride, water, 2.) 50percent NaOH / 1.) benzene, 10 min, 2.) benzene, water, RT, 90 min
2: 72 percent / Triton B / dimethylformamide / 0.75 h
3: 43 percent / H2, K2CO3 / 5percent Pd/C / aq. ethanol / 3 h / 2947.7 Torr
With
sodium hydroxide; water; hydrogen; benzyltrimethylammonium chloride; N-benzyl-trimethylammonium hydroxide; potassium carbonate;
palladium on activated charcoal;
In
ethanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) benzyltrimethylammonium chloride, water, 2.) 50percent NaOH / 1.) benzene, 10 min, 2.) benzene, water, RT, 90 min
2: 72 percent / Triton B / dimethylformamide / 0.75 h
3: 43 percent / H2, K2CO3 / 5percent Pd/C / aq. ethanol / 3 h / 2947.7 Torr
With
sodium hydroxide; water; hydrogen; benzyltrimethylammonium chloride; N-benzyl-trimethylammonium hydroxide; potassium carbonate;
palladium on activated charcoal;
In
ethanol; N,N-dimethyl-formamide;
