ester benzylique de la N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-L-serine

Base Information

Chemical Name:ester benzylique de la N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-L-serine
CAS No.:77870-94-1
Molecular Formula:C₅₂H₅₃NO₁₀
Molecular Weight:851.994
Hs Code.:

Synonyms:ester benzylique de la N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-L-serine

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Chemical Property of ester benzylique de la N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-L-serine

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Technology Process of ester benzylique de la N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-L-serine

There total 12 articles about ester benzylique de la N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-L-serine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21209-51-8
N-benzyloxycarbonyl-L-serine benzyl ester

: 3,5-dimethoxyphenyl 2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside

: 77870-95-2
ester benzylique de la N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-L-serine

: 77870-94-1
ester benzylique de la N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-L-serine

Guidance literature:: With tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; dimesityl(trifluoromethyl)sulfonium trifluoromethanesulfonate; In acetonitrile; at -30 ℃; for 12h; Overall yield = 84 percent; Molecular sieve; Irradiation; Inert atmosphere;
DOI:10.1039/d1cc04473g

Reference yield:

: 38184-10-0
phenyl 2,3,4,5-tetra-O-benzyl-1-thio-β-D-glucopyranoside

: 21209-51-8
N-benzyloxycarbonyl-L-serine benzyl ester

: 77870-95-2
ester benzylique de la N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-L-serine

: 77870-94-1
ester benzylique de la N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-L-serine

Guidance literature:: With iodine; oxygen; In acetonitrile; at 25.1 - 25.9 ℃; for 24h; Overall yield = 36 percent; Overall yield = 49 mg; Schlenk technique; Sealed tube; Irradiation; Green chemistry;
DOI:10.1002/ejoc.201900143

Reference yield:

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: 21209-51-8
N-benzyloxycarbonyl-L-serine benzyl ester

: 77870-95-2
ester benzylique de la N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-L-serine

: 77870-94-1
ester benzylique de la N-(benzyloxycarbonyl)-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-L-serine

Guidance literature:: With trifluoromethanesulfonic acid anhydride; In dichloromethane; acetonitrile; at -20 ℃; for 0.833333h; Yield given. Yields of byproduct given;