Technology Process of genistein 4',7-di-O-(tri-O-benzoyl-6-deoxy-α-L-talopyranoside)
There total 11 articles about genistein 4',7-di-O-(tri-O-benzoyl-6-deoxy-α-L-talopyranoside) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
boron trifluoride diethyl etherate;
In
dichloromethane;
at 0 - 20 ℃;
Molecular sieve;
DOI:10.1002/cjoc.201090291
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrogenchloride; water; zinc(II) chloride / 0 °C / Reflux
2: boron trifluoride diethyl etherate; methanesulfonyl chloride / N,N-dimethyl-formamide / 12 h / 50 °C / Molecular sieve
3: pyridine; 1,1,1,3,3,3-hexamethyl-disilazane / 0.5 h / 20 °C
4: boron trifluoride diethyl etherate / 2 h / 0 - 20 °C
5: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / Molecular sieve
With
pyridine; hydrogenchloride; boron trifluoride diethyl etherate; water; methanesulfonyl chloride; 1,1,1,3,3,3-hexamethyl-disilazane; zinc(II) chloride;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/cjoc.201090291
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0 - 20 °C
2: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / Molecular sieve
With
boron trifluoride diethyl etherate; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
dichloromethane;
DOI:10.1002/cjoc.201090291