6-benzyloxycarbonylamino-hexanoic acid hydrazide

Base Information

• Chemical Name: 6-benzyloxycarbonylamino-hexanoic acid hydrazide
• CAS No.: 115377-84-9
• Molecular Formula: C₁₄H₂₁N₃O₃
• Molecular Weight: 279.339
• Mol file: 115377-84-9.mol

Synonyms:6-benzyloxycarbonylamino-hexanoic acid hydrazide

Chemical Property of 6-benzyloxycarbonylamino-hexanoic acid hydrazide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 6-benzyloxycarbonylamino-hexanoic acid hydrazide

There total 2 articles about 6-benzyloxycarbonylamino-hexanoic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-(benzyloxycarbonylamino)hexanoic acid (1947-00-8) → 6-benzyloxycarbonylamino-hexanoic acid hydrazide (115377-84-9)

Guidance literature:

With chloroformic acid ethyl ester; anschliessend Behandeln mit N₂H₄+H₂O;

Reference yield:

tert-butyl 2-(6-(((benzyloxy)carbonyl)amino)hexanoyl)hydrazine-1-carboxylate → 6-benzyloxycarbonylamino-hexanoic acid hydrazide (115377-84-9)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; dichloromethane;

DOI:10.1021/acs.jmedchem.5b01464

Reference yield: 95.0%

6-benzyloxycarbonylamino-hexanoic acid hydrazide (115377-84-9) → (5-Azidocarbonyl-pentyl)-carbamic acid benzyl ester

Guidance literature:

With nitrosonium tetrafluoroborate; In dichloromethane; for 0.166667h; from -40 gradC to room temperature;

DOI:10.1016/S0040-4039(00)95598-9

upstream raw materials:

6-(benzyloxycarbonylamino)hexanoic acid