2,6-dimethylphenyl fluoroformate

Base Information

• Chemical Name: 2,6-dimethylphenyl fluoroformate
• CAS No.: 153880-74-1
• Molecular Formula: C₉H₉FO₂
• Molecular Weight: 168.168
• Mol file: 153880-74-1.mol

Synonyms:2,6-dimethylphenyl fluoroformate

Chemical Property of 2,6-dimethylphenyl fluoroformate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,6-dimethylphenyl fluoroformate

There total 4 articles about 2,6-dimethylphenyl fluoroformate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2,6-dimethylphenyl chloroformic acid ester (876-99-3) → 2,6-dimethylphenyl fluoroformate (153880-74-1)

Guidance literature:

With potassium fluoride; 18-crown-6 ether; In dichloromethane; for 5h; other reagent: hydrogen fluoride;

DOI:10.1021/jo9716486

Reference yield: 80.0%

→ 2,6-dimethylphenyl fluoroformate (153880-74-1)

Guidance literature:

Reference yield: 68.0%

→ 2-fluoro-m-xylene (443-88-9) + 2,6-dimethylphenyl fluoroformate (153880-74-1)

Guidance literature:

upstream raw materials:

2,6-dimethylphenyl chloroformic acid ester

Downstream raw materials:

2-fluoro-m-xylene

Refernces

• 1、 -. "Process for the preparation of halogenated aromatic compounds". . . Retrieved 2008/06/13.