5-[4-[2-(acryloyloxy)ethoxy]phenyl]-10,15,20-tris(4-pyridyl)porphyrinate zinc(II)

Base Information

Chemical Name:5-[4-[2-(acryloyloxy)ethoxy]phenyl]-10,15,20-tris(4-pyridyl)porphyrinate zinc(II)
CAS No.:1373752-39-6
Molecular Formula:C₄₆H₃₁N₇O₃Zn
Molecular Weight:795.187
Hs Code.:

Synonyms:5-[4-[2-(acryloyloxy)ethoxy]phenyl]-10,15,20-tris(4-pyridyl)porphyrinate zinc(II)

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Chemical Property of 5-[4-[2-(acryloyloxy)ethoxy]phenyl]-10,15,20-tris(4-pyridyl)porphyrinate zinc(II)

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Technology Process of 5-[4-[2-(acryloyloxy)ethoxy]phenyl]-10,15,20-tris(4-pyridyl)porphyrinate zinc(II)

There total 3 articles about 5-[4-[2-(acryloyloxy)ethoxy]phenyl]-10,15,20-tris(4-pyridyl)porphyrinate zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 5-[4-[2-(acryloyloxy)ethoxy]phenyl]-10,15,20-tris(4-pyridyl)porphyrin

: 1373752-39-6
5-[4-[2-(acryloyloxy)ethoxy]phenyl]-10,15,20-tris(4-pyridyl)porphyrinate zinc(II)

Guidance literature:: With zinc diacetate; In methanol; chloroform; at 20 ℃; for 2h;
DOI:10.1016/j.jphotochem.2011.03.020

Reference yield:

: 872-85-5
pyridine-4-carbaldehyde

: 1373752-39-6
5-[4-[2-(acryloyloxy)ethoxy]phenyl]-10,15,20-tris(4-pyridyl)porphyrinate zinc(II)

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic anhydride / 3 h / Reflux

2.1: sodium hydroxide / N,N-dimethyl-formamide / 1.5 h / 20 °C / Inert atmosphere

2.2: 3 h / 20 °C / Inert atmosphere

3.1: zinc diacetate / methanol; chloroform / 2 h / 20 °C

With zinc diacetate; acetic anhydride; sodium hydroxide; In methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/j.jphotochem.2011.03.020

Reference yield:

: 4823-47-6
acrylic acid 2-bromoethyl ester

: 5-<4-<(Ethylcarbonyl)oxy>phenyl>-10,15,20-tris-(4-pyridyl)porphyrin

: 1373752-39-6
5-[4-[2-(acryloyloxy)ethoxy]phenyl]-10,15,20-tris(4-pyridyl)porphyrinate zinc(II)

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / N,N-dimethyl-formamide / 1.5 h / 20 °C / Inert atmosphere

1.2: 3 h / 20 °C / Inert atmosphere

2.1: zinc diacetate / methanol; chloroform / 2 h / 20 °C

With zinc diacetate; sodium hydroxide; In methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/j.jphotochem.2011.03.020