(R)-3-(1-Phenyl-cycloheptanecarbonyloxy)-1-(3-pyridin-4-yl-propyl)-1-azonia-bicyclo[2.2.2]octane bromide

Base Information

Chemical Name:(R)-3-(1-Phenyl-cycloheptanecarbonyloxy)-1-(3-pyridin-4-yl-propyl)-1-azonia-bicyclo[2.2.2]octane bromide
CAS No.:1196091-89-0
Molecular Formula:Br*C₂₉H₃₉N₂O₂
Molecular Weight:527.545
Hs Code.:

Synonyms:(R)-3-(1-Phenyl-cycloheptanecarbonyloxy)-1-(3-pyridin-4-yl-propyl)-1-azonia-bicyclo[2.2.2]octane bromide

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Chemical Property of (R)-3-(1-Phenyl-cycloheptanecarbonyloxy)-1-(3-pyridin-4-yl-propyl)-1-azonia-bicyclo[2.2.2]octane bromide

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Technology Process of (R)-3-(1-Phenyl-cycloheptanecarbonyloxy)-1-(3-pyridin-4-yl-propyl)-1-azonia-bicyclo[2.2.2]octane bromide

There total 11 articles about (R)-3-(1-Phenyl-cycloheptanecarbonyloxy)-1-(3-pyridin-4-yl-propyl)-1-azonia-bicyclo[2.2.2]octane bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1026791-31-0
1-phenyl-cycloheptanecarboxylic acid (R)-(1-aza-bicyclo[2.2.2]oct-3-yl)ester

: 64262-18-6
4-(3-bromopropyl)pyridine hydrobromide

: 1196091-89-0
(R)-3-(1-Phenyl-cycloheptanecarbonyloxy)-1-(3-pyridin-4-yl-propyl)-1-azonia-bicyclo[2.2.2]octane bromide

Guidance literature:: 4-(3-bromopropyl)pyridine hydrobromide; With sodium hydroxide; In diethyl ether;

1-phenyl-cycloheptanecarboxylic acid (R)-(1-aza-bicyclo[2.2.2]oct-3-yl)ester; In acetonitrile; for 48h;

Reference yield:

: 7278-77-5
(1-chloro-cycloheptyl)-phenyl-methanone

: 1196091-89-0
(R)-3-(1-Phenyl-cycloheptanecarbonyloxy)-1-(3-pyridin-4-yl-propyl)-1-azonia-bicyclo[2.2.2]octane bromide

Guidance literature:: Multi-step reaction with 4 steps

1.1: water / silver nitrate / 1,4-dioxane / 4.5 h / 75 °C

2.1: trimethylsilyldiazomethane / toluene / 0.75 h / Inert atmosphere

3.1: toluene / 0.5 h / Reflux

3.2: Inert atmosphere; Reflux

4.1: sodium hydroxide / diethyl ether

4.2: 48 h

With water; trimethylsilyldiazomethane; sodium hydroxide; silver nitrate; In 1,4-dioxane; diethyl ether; toluene;

Reference yield:

: 6004-52-0
cycloheptyl(phenyl)methanone

: 1196091-89-0
(R)-3-(1-Phenyl-cycloheptanecarbonyloxy)-1-(3-pyridin-4-yl-propyl)-1-azonia-bicyclo[2.2.2]octane bromide

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuryl dichloride / 1 h / 0 °C

1.2: Reflux

2.1: water / silver nitrate / 1,4-dioxane / 4.5 h / 75 °C

3.1: trimethylsilyldiazomethane / toluene / 0.75 h / Inert atmosphere

4.1: toluene / 0.5 h / Reflux

4.2: Inert atmosphere; Reflux

5.1: sodium hydroxide / diethyl ether

5.2: 48 h

With sulfuryl dichloride; water; trimethylsilyldiazomethane; sodium hydroxide; silver nitrate; In 1,4-dioxane; diethyl ether; toluene;