Acetic acid (R)-3-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-4-methyl-pentyl ester

Base Information

Chemical Name:Acetic acid (R)-3-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-4-methyl-pentyl ester
CAS No.:124484-44-2
Molecular Formula:C₂₆H₃₈O₃Si
Molecular Weight:426.671
Hs Code.:

Synonyms:Acetic acid (R)-3-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-4-methyl-pentyl ester

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Chemical Property of Acetic acid (R)-3-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-4-methyl-pentyl ester

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Technology Process of Acetic acid (R)-3-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-4-methyl-pentyl ester

There total 6 articles about Acetic acid (R)-3-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-4-methyl-pentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 124469-35-8
(R)-5-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-6-methyl-heptan-2-one

: 124484-44-2
Acetic acid (R)-3-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-4-methyl-pentyl ester

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; for 48h; Heating;
DOI:10.1016/S0040-4039(01)01964-5

Reference yield:

: 5989-27-5,555-08-8,8022-90-0,9003-73-0,95327-98-3
D-limonene

: 124484-44-2
Acetic acid (R)-3-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-4-methyl-pentyl ester

Guidance literature:: Multi-step reaction with 6 steps

1.1: H₂ / PtO₂ / methanol

2.1: O₃ / CH₂Cl₂; methanol / 1 h / -60 °C

2.2: p-TsOH / methanol / 1 h / -60 - 0 °C

3.1: 100 percent / HClO₄ / H₂O; tetrahydrofuran

4.1: 98 percent / lithium tris[(3-ethyl-3-pentyl)oxy]aluminohydride / tetrahydrofuran / 1 h / -78 °C

5.1: 96 percent / DBU / CH₂Cl₂

6.1: 100 percent / MCPBA / CHCl₃ / 48 h / Heating

With perchloric acid; Lithium tris[(3-ethyl-3-pentyl)-oxy]aluminohydride; hydrogen; ozone; 1,8-diazabicyclo[5.4.0]undec-7-ene; 3-chloro-benzenecarboperoxoic acid; platinum(IV) oxide; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; 6.1: Baeyer-Villiger reaction;
DOI:10.1016/S0040-4039(01)01964-5

Reference yield:

: 67304-08-9
(R)-3-isopropyl-6-oxoheptanal

: 124484-44-2
Acetic acid (R)-3-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-4-methyl-pentyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / lithium tris[(3-ethyl-3-pentyl)oxy]aluminohydride / tetrahydrofuran / 1 h / -78 °C

2: 96 percent / DBU / CH₂Cl₂

3: 100 percent / MCPBA / CHCl₃ / 48 h / Heating

With Lithium tris[(3-ethyl-3-pentyl)-oxy]aluminohydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; chloroform; 3: Baeyer-Villiger reaction;
DOI:10.1016/S0040-4039(01)01964-5