2-N-acetyl-9-(2-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-β-D-ribofuranosyl)-6-O-diphenylcarbamoylguanine

Base Information

• Chemical Name: 2-N-acetyl-9-(2-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-β-D-ribofuranosyl)-6-O-diphenylcarbamoylguanine
• CAS No.: 959843-70-0
• Molecular Formula: C₃₅H₃₂N₆O₈
• Molecular Weight: 664.674

Synonyms:2-N-acetyl-9-(2-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-β-D-ribofuranosyl)-6-O-diphenylcarbamoylguanine

Chemical Property of 2-N-acetyl-9-(2-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-β-D-ribofuranosyl)-6-O-diphenylcarbamoylguanine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2-N-acetyl-9-(2-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-β-D-ribofuranosyl)-6-O-diphenylcarbamoylguanine

There total 2 articles about 2-N-acetyl-9-(2-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-β-D-ribofuranosyl)-6-O-diphenylcarbamoylguanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-D-ribofuranose (444019-07-2) + N2-acetyl-O6-(diphenylcarbamoyl)guanine (112233-74-6) → 2-N-acetyl-9-N2-(2-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-β-D-ribofuranosyl)-6-O-diphenylcarbamoylguanine + 2-N-acetyl-9-(2-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-β-D-ribofuranosyl)-6-O-diphenylcarbamoylguanine (959843-70-0)

Guidance literature:

N₂-acetyl-O₆-(diphenylcarbamoyl)guanine; With benzenesulfonamide; In 1,2-dichloro-ethane; at 80 ℃; for 1h;

1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-D-ribofuranose; With trimethylsilyl trifluoromethanesulfonate; In toluene; at 0 - 80 ℃;

With sodium hydrogencarbonate; In ethyl acetate; toluene; Further stages.;

DOI:10.1016/j.tet.2007.08.092

Reference yield: 55.0%

1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-D-ribofuranose (444019-07-2) + N2-acetyl-O6-(diphenylcarbamoyl)guanine (112233-74-6) → 2-N-acetyl-9-(2-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-β-D-ribofuranosyl)-6-O-diphenylcarbamoylguanine (959843-70-0)

Guidance literature:

N₂-acetyl-O₆-(diphenylcarbamoyl)guanine; With N,O-bis-(trimethylsilyl)-acetamide;

1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-D-ribofuranose; With trimethylsilyl trifluoromethanesulfonate; Further stages.;

DOI:10.1080/15257770701521730

Reference yield: 90.0%

2-N-acetyl-9-(2-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-β-D-ribofuranosyl)-6-O-diphenylcarbamoylguanine (959843-70-0) → 9-(5-O-benzoyl-3-deoxy-3-C-methyl-β-D-ribofuranosyl)-N2-acetylguanine (1065271-34-2)

Guidance literature:

With pyridine; hydrazine hydrate; acetic acid; at 20 ℃; for 120h;

DOI:10.1016/j.bmc.2008.06.011

upstream raw materials:

1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3-C-methyl-D-ribofuranose

N₂-acetyl-O₆-(diphenylcarbamoyl)guanine

Downstream raw materials:

C₁₈H₁₉N₅O₄

9-(5-O-benzoyl-3-deoxy-3-C-methyl-β-D-ribofuranosyl)-N²-acetylguanine

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