C₃₃H₂₄BF₂I₃N₂

Base Information

• Chemical Name: C₃₃H₂₄BF₂I₃N₂
• CAS No.: 1257341-75-5
• Molecular Formula: C₃₃H₂₄BF₂I₃N₂
• Molecular Weight: 878.088
• Mol file: 1257341-75-5.mol

Synonyms:C₃₃H₂₄BF₂I₃N₂

Chemical Property of C₃₃H₂₄BF₂I₃N₂

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₃H₂₄BF₂I₃N₂

There total 1 articles about C₃₃H₂₄BF₂I₃N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

p-(iodophenyl)carboxaldehyde (15164-44-0) + 4,4-difluoro-8-(4'-iodophenyl)-1,3,5,7-tetramethyl-4-bora-3a,4a-diaza-s-indacene → C33H24BF2I3N2 (1257341-75-5)

Guidance literature:

With piperidine; toluene-4-sulfonic acid; In toluene; at 140 ℃; for 0.166667h;

DOI:10.1055/s-0030-1258050

Reference yield: 94.0%

3-(2-methoxyethoxy)prop-1-yne (31995-08-1) + C33H24BF2I3N2 (1257341-75-5) → C45H42BI3N2O4 (1257341-79-9)

Guidance literature:

With ethylmagnesium bromide; In tetrahydrofuran; at 60 ℃;

DOI:10.1055/s-0030-1258050

Reference yield: 85.0%

ethyl hept-6-ynoate (105339-02-4) + C33H24BF2I3N2 (1257341-75-5) → C60H63BF2N2O6 (1257341-81-3)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; In benzene; at 80 ℃; for 15h;

DOI:10.1055/s-0030-1258050

upstream raw materials:

p-(iodophenyl)carboxaldehyde

Downstream raw materials:

C₆₀H₆₃BF₂N₂O₆

C₄₅H₄₂BI₃N₂O₄