2,2-dimethylpropionic acid 13-(1-phenyl-1H-tetrazole-5-sulfonyl)tridecyl ester

Base Information

• Chemical Name: 2,2-dimethylpropionic acid 13-(1-phenyl-1H-tetrazole-5-sulfonyl)tridecyl ester
• CAS No.: 1204202-24-3
• Molecular Formula: C₂₅H₄₀N₄O₄S
• Molecular Weight: 492.683

Synonyms:2,2-dimethylpropionic acid 13-(1-phenyl-1H-tetrazole-5-sulfonyl)tridecyl ester

Chemical Property of 2,2-dimethylpropionic acid 13-(1-phenyl-1H-tetrazole-5-sulfonyl)tridecyl ester

Chemical Property:

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Technology Process of 2,2-dimethylpropionic acid 13-(1-phenyl-1H-tetrazole-5-sulfonyl)tridecyl ester

There total 3 articles about 2,2-dimethylpropionic acid 13-(1-phenyl-1H-tetrazole-5-sulfonyl)tridecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

13-((1-phenyl-1H-tetrazol-5-yl)thio)tridecyl pivaloate → 2,2-dimethylpropionic acid 13-(1-phenyl-1H-tetrazole-5-sulfonyl)tridecyl ester (1204202-24-3)

Guidance literature:

With hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide; In tetrahydrofuran; at 20 ℃; for 20h; Cooling with ice;

DOI:10.1016/j.tet.2016.08.089

Reference yield:

13-bromotridecyl pivaloate → 2,2-dimethylpropionic acid 13-(1-phenyl-1H-tetrazole-5-sulfonyl)tridecyl ester (1204202-24-3)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 18 h / 20 °C

2: hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide / tetrahydrofuran / 20 h / 20 °C / Cooling with ice

With hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide; potassium carbonate; In tetrahydrofuran; acetone;

DOI:10.1016/j.tet.2016.08.089

Reference yield:

(E/Z)-13-bromotridec-7-en-1-yl pivaloate → 2,2-dimethylpropionic acid 13-(1-phenyl-1H-tetrazole-5-sulfonyl)tridecyl ester (1204202-24-3)

Guidance literature:

Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / 1 h

2: potassium carbonate / acetone / 18 h / 20 °C

3: hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide / tetrahydrofuran / 20 h / 20 °C / Cooling with ice

With palladium 10% on activated carbon; hexaammonium heptamolybdate tetrahydrate; hydrogen; dihydrogen peroxide; potassium carbonate; In tetrahydrofuran; acetone;

DOI:10.1016/j.tet.2016.08.089

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