3-FLUORO-4-(TRIFLUOROMETHYL)PHENACYL BROMIDE

Base Information

• Chemical Name: 3-FLUORO-4-(TRIFLUOROMETHYL)PHENACYL BROMIDE
• CAS No.: 544429-22-3
• Molecular Formula: C₉H₅BrF₄O
• Molecular Weight: 285.036
• Hs Code.: 2914790090
• Mol file: 544429-22-3.mol

Synonyms:2-bromo-1-(3-fluoro-4-(trifluoromethyl)phenyl)ethan-1-one

Chemical Property of 3-FLUORO-4-(TRIFLUOROMETHYL)PHENACYL BROMIDE

Chemical Property:

• Melting Point: 29-31
• Storage Temp.: Keep Cold
• Sensitive.: Lachrymatory

Purity/Quality:

98% ^*data from raw suppliers

3-fluoro-4-(trifluormethyl)phenacylbromide 95 ^*data from reagent suppliers

Safty Information:

• Hazard Codes: C

MSDS Files:

Useful:

Technology Process of 3-FLUORO-4-(TRIFLUOROMETHYL)PHENACYL BROMIDE

There total 1 articles about 3-FLUORO-4-(TRIFLUOROMETHYL)PHENACYL BROMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(3-fluoro-4-(trifluoromethyl)phenyl)ethan-1-one (237761-81-8) → 2-bromo-1-(3-fluoro-4-(trifluoromethyl)phenyl)ethan-1-one (544429-22-3)

Guidance literature:

With copper(ll) bromide; In ethyl acetate; at 20 - 80 ℃; for 4h; Inert atmosphere;

Reference yield:

2-bromo-1-(3-fluoro-4-(trifluoromethyl)phenyl)ethan-1-one (544429-22-3) + (E,Z)-5-bromo-N′-hydroxy-6-methoxypicolinimidamide → (Z)-5-bromo-N’-(2-(3-fluoro-4-(trifluoromethyl)phenyl)-2-oxoethoxy)-6-methoxypicolinimidamide

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 - 80 ℃; for 0.333333h; Inert atmosphere; Microwave irradiation;

Reference yield:

2-bromo-1-(3-fluoro-4-(trifluoromethyl)phenyl)ethan-1-one (544429-22-3) + diethyl 4-cyclopropyl-1H-pyrazole-3,5-dicarboxylate → diethyl 4-cyclopropyl-1-{2-[3-fluoro-4-(trifluoromethyl)phenyl]-2-oxoethyl}-1H-pyrazole-3,5-dicarboxylate

Guidance literature:

With potassium carbonate; In acetone; at 20 ℃; for 2h;

upstream raw materials:

1-(3-fluoro-4-(trifluoromethyl)phenyl)ethan-1-one

Downstream raw materials:

N-{4-[3-fluoro-4-(trifluoromethyl)phenyl]-1H-imidazol-2-yl}acetamide

Refernces