Technology Process of C25H27N
There total 3 articles about C25H27N which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate;
In
methanol;
at 20 ℃;
for 15h;
Inert atmosphere;
Schlenk technique;
DOI:10.1021/om301063n
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 °C / Inert atmosphere; Schlenk technique
1.2: 16 h / 0 - 20 °C / Inert atmosphere; Schlenk technique
2.1: lithium aluminium tetrahydride / diethyl ether / 17 h / 0 - 50 °C / Inert atmosphere; Schlenk technique
3.1: methanol / 4 h / 20 °C
4.1: sodium tetrahydroborate / methanol / 15 h / 20 °C / Inert atmosphere; Schlenk technique
With
sodium tetrahydroborate; lithium aluminium tetrahydride; sodium hydride;
In
tetrahydrofuran; methanol; diethyl ether; mineral oil;
1.2: |Tsuji-Trost Allylation;
DOI:10.1021/om301063n
- Guidance literature:
-
Multi-step reaction with 2 steps
1: methanol / 4 h / 20 °C
2: sodium tetrahydroborate / methanol / 15 h / 20 °C / Inert atmosphere; Schlenk technique
With
sodium tetrahydroborate;
In
methanol;
DOI:10.1021/om301063n