(S)-2-(Naphthalene-1-sulfonylamino)-5-phenyl-pentanoic acid (3-carbamimidoyl-phenyl)-amide; hydriodide

Base Information

Chemical Name:(S)-2-(Naphthalene-1-sulfonylamino)-5-phenyl-pentanoic acid (3-carbamimidoyl-phenyl)-amide; hydriodide
CAS No.:90291-98-8
Molecular Formula:C₂₈H₂₈N₄O₃S*HI
Molecular Weight:628.534
Hs Code.:

Synonyms:(S)-2-(Naphthalene-1-sulfonylamino)-5-phenyl-pentanoic acid (3-carbamimidoyl-phenyl)-amide; hydriodide

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Chemical Property of (S)-2-(Naphthalene-1-sulfonylamino)-5-phenyl-pentanoic acid (3-carbamimidoyl-phenyl)-amide; hydriodide

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Technology Process of (S)-2-(Naphthalene-1-sulfonylamino)-5-phenyl-pentanoic acid (3-carbamimidoyl-phenyl)-amide; hydriodide

There total 7 articles about (S)-2-(Naphthalene-1-sulfonylamino)-5-phenyl-pentanoic acid (3-carbamimidoyl-phenyl)-amide; hydriodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 90291-87-5
3-[2-(Naphthalene-1-sulfonylamino)-5-phenyl-pentanoylamino]-thiobenzimidic acid methyl ester; hydriodide

: 90291-98-8
(S)-2-(Naphthalene-1-sulfonylamino)-5-phenyl-pentanoic acid (3-carbamimidoyl-phenyl)-amide; hydriodide

Guidance literature:: With ammonium acetate; In ethanol; at 60 ℃; for 2.5h;

Reference yield:

: 85-46-1
1-Naphthalenesulfonyl chloride

: 90291-98-8
(S)-2-(Naphthalene-1-sulfonylamino)-5-phenyl-pentanoic acid (3-carbamimidoyl-phenyl)-amide; hydriodide

Guidance literature:: Multi-step reaction with 6 steps

1: 78 percent / 1 mol/l NaOH / diethyl ether; H₂O

2: SOCl₂ / 1 h / Heating

3: 51 percent / TEA / benzene / 1.5 h

4: 98 percent / H₂S, TEA / pyridine / Ambient temperature

5: 75 percent / acetone / 20 h / Ambient temperature

6: 72 percent / NH₄COOCH₃ / ethanol / 2.5 h / 60 °C

With sodium hydroxide; thionyl chloride; TEA; hydrogen sulfide; ammonium acetate; In pyridine; diethyl ether; ethanol; water; acetone; benzene;

Reference yield:

: 34993-02-7,2046-19-7
2-(R)-amino-5-phenylpentanoic acid

: 90291-98-8
(S)-2-(Naphthalene-1-sulfonylamino)-5-phenyl-pentanoic acid (3-carbamimidoyl-phenyl)-amide; hydriodide

Guidance literature:: Multi-step reaction with 6 steps

1: 78 percent / 1 mol/l NaOH / diethyl ether; H₂O

2: SOCl₂ / 1 h / Heating

3: 51 percent / TEA / benzene / 1.5 h

4: 98 percent / H₂S, TEA / pyridine / Ambient temperature

5: 75 percent / acetone / 20 h / Ambient temperature

6: 72 percent / NH₄COOCH₃ / ethanol / 2.5 h / 60 °C

With sodium hydroxide; thionyl chloride; TEA; hydrogen sulfide; ammonium acetate; In pyridine; diethyl ether; ethanol; water; acetone; benzene;