6-O-(4-O-((R)-3-azido-2-((R)-3-azido-2-O-hydroxypropyl)propyl)-2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl)-1-N-[(S)-2-O-benzyl-4-(benzyloxycarbonylamino)butanosyl]-3,2',6'-triazidoneamine

Base Information

• Chemical Name: 6-O-(4-O-((R)-3-azido-2-((R)-3-azido-2-O-hydroxypropyl)propyl)-2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl)-1-N-[(S)-2-O-benzyl-4-(benzyloxycarbonylamino)butanosyl]-3,2',6'-triazidoneamine
• CAS No.: 1055042-37-9
• Molecular Formula: C₆₄H₇₇N₁₇O₁₆
• Molecular Weight: 1340.42

Synonyms:6-O-(4-O-((R)-3-azido-2-((R)-3-azido-2-O-hydroxypropyl)propyl)-2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl)-1-N-[(S)-2-O-benzyl-4-(benzyloxycarbonylamino)butanosyl]-3,2',6'-triazidoneamine

Chemical Property of 6-O-(4-O-((R)-3-azido-2-((R)-3-azido-2-O-hydroxypropyl)propyl)-2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl)-1-N-[(S)-2-O-benzyl-4-(benzyloxycarbonylamino)butanosyl]-3,2',6'-triazidoneamine

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Technology Process of 6-O-(4-O-((R)-3-azido-2-((R)-3-azido-2-O-hydroxypropyl)propyl)-2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl)-1-N-[(S)-2-O-benzyl-4-(benzyloxycarbonylamino)butanosyl]-3,2',6'-triazidoneamine

There total 1 articles about 6-O-(4-O-((R)-3-azido-2-((R)-3-azido-2-O-hydroxypropyl)propyl)-2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl)-1-N-[(S)-2-O-benzyl-4-(benzyloxycarbonylamino)butanosyl]-3,2',6'-triazidoneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C68H81N17O18 → 6-O-(4-O-((R)-3-azido-2-((R)-3-azido-2-O-hydroxypropyl)propyl)-2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl)-1-N-[(S)-2-O-benzyl-4-(benzyloxycarbonylamino)butanosyl]-3,2',6'-triazidoneamine (1055042-37-9)

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 24h;

DOI:10.1021/jo062588j

Reference yield:

6-O-(4-O-((R)-3-azido-2-((R)-3-azido-2-O-hydroxypropyl)propyl)-2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl)-1-N-[(S)-2-O-benzyl-4-(benzyloxycarbonylamino)butanosyl]-3,2',6'-triazidoneamine (1055042-37-9) → C64H87N7O16

Guidance literature:

With sodium hydroxide; trimethylphosphane; In tetrahydrofuran; at 50 ℃; for 2h;

DOI:10.1021/jo062588j

Reference yield:

6-O-(4-O-((R)-3-azido-2-((R)-3-azido-2-O-hydroxypropyl)propyl)-2,3-di-O-benzyl-6-deoxy-α-D-glucopyranosyl)-1-N-[(S)-2-O-benzyl-4-(benzyloxycarbonylamino)butanosyl]-3,2',6'-triazidoneamine (1055042-37-9) → 6-O-(4-O-((R)-3-amino-2-((R)-3-amino-2-hydroxypropyl)-propyl)-6-deoxy-α-D-glucopyranosyl)-1-N-[(S)-4-amino-2-hydroxybutanoyl]neamine hexahydrochloride

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaOH; PMe₃ / tetrahydrofuran / 2 h / 50 °C

2: H₂; AcOH / Pd(OH)2/C / H₂O / 24 h / 20 °C / atmospheric pressure

With sodium hydroxide; hydrogen; acetic acid; trimethylphosphane; palladium dihydroxide; In tetrahydrofuran; water;

DOI:10.1021/jo062588j

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