N-[(phenylthio)acetyl]decaquinoline

Base Information

• Chemical Name: N-[(phenylthio)acetyl]decaquinoline
• CAS No.: 1224199-41-0
• Molecular Formula: C₁₇H₂₃NOS
• Molecular Weight: 289.442
• Mol file: 1224199-41-0.mol

Synonyms:N-[(phenylthio)acetyl]decaquinoline

Chemical Property of N-[(phenylthio)acetyl]decaquinoline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-[(phenylthio)acetyl]decaquinoline

There total 1 articles about N-[(phenylthio)acetyl]decaquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(phenylthio)acetic acid (103-04-8) + decahydroquinoline (767-92-0,10343-99-4,22160-37-8,22160-38-9,105728-23-2,115730-30-8,115730-31-9,150254-00-5,2051-28-7) → N-[(phenylthio)acetyl]decaquinoline (1224199-41-0)

Guidance literature:

(phenylthio)acetic acid; decahydroquinoline; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

With hydrogenchloride; In water; N,N-dimethyl-formamide; pH=4; Cooling with ice;

Reference yield:

N-[(phenylthio)acetyl]decaquinoline (1224199-41-0) → N-(2-phenylthio)ethyldecahydroquinoline hydrochloride

Guidance literature:

N-[(phenylthio)acetyl]decaquinoline; With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 - 40 ℃; Inert atmosphere; Cooling with ice;

With Glauber's salt; at 20 ℃; for 4h; Cooling with ice;

With hydrogenchloride; In hexane; ethyl acetate; at 20 ℃;

upstream raw materials:

(phenylthio)acetic acid

decahydroquinoline