cis-(2R,4R)-2-<<2-<<<(1,1-dimethylethyl)dimethylsilyl>oxy>methyl>-1-prop-2-enyl>oxy>-4-methyl-1-methylenecyclohexane

Base Information

Chemical Name:cis-(2R,4R)-2-<<2-<<<(1,1-dimethylethyl)dimethylsilyl>oxy>methyl>-1-prop-2-enyl>oxy>-4-methyl-1-methylenecyclohexane
CAS No.:145668-29-7
Molecular Formula:C₁₈H₃₄O₂Si
Molecular Weight:310.552
Hs Code.:

Synonyms:cis-(2R,4R)-2-<<2-<<<(1,1-dimethylethyl)dimethylsilyl>oxy>methyl>-1-prop-2-enyl>oxy>-4-methyl-1-methylenecyclohexane

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Chemical Property of cis-(2R,4R)-2-<<2-<<<(1,1-dimethylethyl)dimethylsilyl>oxy>methyl>-1-prop-2-enyl>oxy>-4-methyl-1-methylenecyclohexane

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Technology Process of cis-(2R,4R)-2-<<2-<<<(1,1-dimethylethyl)dimethylsilyl>oxy>methyl>-1-prop-2-enyl>oxy>-4-methyl-1-methylenecyclohexane

There total 4 articles about cis-(2R,4R)-2-<<2-<<<(1,1-dimethylethyl)dimethylsilyl>oxy>methyl>-1-prop-2-enyl>oxy>-4-methyl-1-methylenecyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22472-80-6
syn-(-)-pulegol

: 145668-29-7
cis-(2R,4R)-2-<<2-<<<(1,1-dimethylethyl)dimethylsilyl>oxy>methyl>-1-prop-2-enyl>oxy>-4-methyl-1-methylenecyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) O₃, 2.) Me₂S

2: 1.) tBuOK / 1.) THF

3: 1.) NaH, 2.) tetrabutylammonium iodide / 1.) THF, 62 deg C, 1,5 h, 2.) THF, 62 deg C, 20 h

With dimethylsulfide; potassium tert-butylate; tetra-(n-butyl)ammonium iodide; sodium hydride; ozone;
DOI:10.1021/jo00056a013

Reference yield:

: 175775-26-5
(2R,4R)-2-hydroxy-4-methylcyclohexanone

: 145668-29-7
cis-(2R,4R)-2-<<2-<<<(1,1-dimethylethyl)dimethylsilyl>oxy>methyl>-1-prop-2-enyl>oxy>-4-methyl-1-methylenecyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) tBuOK / 1.) THF

2: 1.) NaH, 2.) tetrabutylammonium iodide / 1.) THF, 62 deg C, 1,5 h, 2.) THF, 62 deg C, 20 h

With potassium tert-butylate; tetra-(n-butyl)ammonium iodide; sodium hydride;
DOI:10.1021/jo00056a013

Reference yield:

: 145668-28-6
2-(tert-butyldimethylsilyloxy)methyl-3-chloroprop-1-ene

: 145773-23-5
cis-(1R,3R)-3-methyl-6-methylenecyclohexanol

: 145668-29-7
cis-(2R,4R)-2-<<2-<<<(1,1-dimethylethyl)dimethylsilyl>oxy>methyl>-1-prop-2-enyl>oxy>-4-methyl-1-methylenecyclohexane

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; Yield given. Multistep reaction; 1.) THF, 62 deg C, 1,5 h, 2.) THF, 62 deg C, 20 h;
DOI:10.1021/jo00056a013