1-Chlor-2-phenyl-6,7-dihydro-3H,5H-benzochinolizin-3-on

Base Information

• Chemical Name: 1-Chlor-2-phenyl-6,7-dihydro-3H,5H-benzochinolizin-3-on
• CAS No.: 57625-54-4
• Molecular Formula: C₁₈H₁₄ClNO
• Molecular Weight: 295.768

Synonyms:1-Chlor-2-phenyl-6,7-dihydro-3H,5H-benzochinolizin-3-on

Chemical Property of 1-Chlor-2-phenyl-6,7-dihydro-3H,5H-benzochinolizin-3-on

Chemical Property:

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Technology Process of 1-Chlor-2-phenyl-6,7-dihydro-3H,5H-benzochinolizin-3-on

There total 2 articles about 1-Chlor-2-phenyl-6,7-dihydro-3H,5H-benzochinolizin-3-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

4-hydroxy-3-phenyl-1-azatricyclo[7.3.1.05,13]trideca-3,5,7,9(13)-tetraen-2-one (57625-49-7) → 1-Chlor-2-phenyl-6,7-dihydro-3H,5H-benzochinolizin-3-on (57625-54-4)

Guidance literature:

With trichlorophosphate; for 2h; Heating;

DOI:10.1007/BF00809016

Reference yield:

→ 1-Chlor-2-phenyl-6,7-dihydro-3H,5H-benzochinolizin-3-on (57625-54-4)

Guidance literature:

entspr. Dion, PCl5;

Reference yield: 92.0%

1-Chlor-2-phenyl-6,7-dihydro-3H,5H-benzochinolizin-3-on (57625-54-4) + potassium cyanide (151-50-8) → 3-oxo-2-phenyl-6,7-dihydro-3H,5H-benzo[ij]quinolizin-1-carbonitrile (685895-21-0)

Guidance literature:

With sodium 4-methylbenzenesulfinate; In N,N-dimethyl-formamide; at 120 ℃; for 20h;

DOI:10.1002/ejoc.200700855

upstream raw materials:

4-hydroxy-3-phenyl-1-azatricyclo[7.3.1.0^5,13]trideca-3,5,7,9⁽¹³⁾-tetraen-2-one

Downstream raw materials:

1-Amino-2-phenyl-6,7-dihydro-3H,5H-benzochinolizin-3-on

3-oxo-2-phenyl-6,7-dihydro-3H,5H-benzo[ij]quinolizin-1-carbonitrile

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