2-Acetoxy-4-(6',6'-dimethyl-2'-trideuteriomethyl-1'-cyclohexen-1'-yl)butan

Base Information

Chemical Name:2-Acetoxy-4-(6',6'-dimethyl-2'-trideuteriomethyl-1'-cyclohexen-1'-yl)butan
CAS No.:74055-26-8
Molecular Formula:C₁₅H₂₆O₂
Molecular Weight:241.346
Hs Code.:

Synonyms:2-Acetoxy-4-(6',6'-dimethyl-2'-trideuteriomethyl-1'-cyclohexen-1'-yl)butan

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Chemical Property of 2-Acetoxy-4-(6',6'-dimethyl-2'-trideuteriomethyl-1'-cyclohexen-1'-yl)butan

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Technology Process of 2-Acetoxy-4-(6',6'-dimethyl-2'-trideuteriomethyl-1'-cyclohexen-1'-yl)butan

There total 4 articles about 2-Acetoxy-4-(6',6'-dimethyl-2'-trideuteriomethyl-1'-cyclohexen-1'-yl)butan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 74055-25-7
2-Acetoxy-4-(2'-hydroxy-6',6'-dimethyl-2'-trideuteriomethyl-1'-cyclohexyl)butan

: 74055-26-8
2-Acetoxy-4-(6',6'-dimethyl-2'-trideuteriomethyl-1'-cyclohexen-1'-yl)butan

Guidance literature:: With trichlorophosphate; In pyridine; at 96 ℃; for 20h;
DOI:10.1002/hlca.19800630116

Reference yield:

: 13720-13-3
4-(6',6'-dimethyl-2'-methylenecyclohexyl)butan-2-ol

: 74055-26-8
2-Acetoxy-4-(6',6'-dimethyl-2'-trideuteriomethyl-1'-cyclohexen-1'-yl)butan

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / pyridine

2: 98 percent / O₃ / CH₂Cl₂ / -78 °C

3: 1.) Mg, / 1.) ether, 0 deg C, 2.) 0 deg C, 2 h

4: 95 percent / POCl₃ / pyridine / 20 h / 96 °C

With pyridine; ozone; magnesium; trichlorophosphate; In pyridine; dichloromethane;
DOI:10.1002/hlca.19800630116

Reference yield:

: 68479-99-2
2-Acetoxy-4-(2',2'-dimethyl-6'-methyliden-1'-cyclohexyl)butan

: 74055-26-8
2-Acetoxy-4-(6',6'-dimethyl-2'-trideuteriomethyl-1'-cyclohexen-1'-yl)butan

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / O₃ / CH₂Cl₂ / -78 °C

2: 1.) Mg, / 1.) ether, 0 deg C, 2.) 0 deg C, 2 h

3: 95 percent / POCl₃ / pyridine / 20 h / 96 °C

With ozone; magnesium; trichlorophosphate; In pyridine; dichloromethane;
DOI:10.1002/hlca.19800630116