4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl dimethylcarbamate

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Chemical Name:4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl dimethylcarbamate
CAS No.:1224949-11-4
Molecular Formula:C₂₆H₃₁N₃O₄
Molecular Weight:449.55
Hs Code.:

Synonyms:4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl dimethylcarbamate

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Chemical Property of 4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl dimethylcarbamate

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Technology Process of 4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl dimethylcarbamate

There total 8 articles about 4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl dimethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 1224948-06-4
1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)cyclohexane-cis-1,4-diol

: 79-44-7
N,N-Dimethylcarbamoyl chloride

: 1224949-11-4
4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl dimethylcarbamate

Guidance literature:: 1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)cyclohexane-cis-1,4-diol; With sodium hydride; In tetrahydrofuran; for 0.333333h; Cooling with ice;

N,N-Dimethylcarbamoyl chloride; In tetrahydrofuran; at 20 ℃; for 3h;

Reference yield:

: 1224949-51-2
8-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-1,4-dioxaspiro[4.5]decan-8-ol

: 1224949-11-4
4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl dimethylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; water / tetrahydrofuran / 15 h / 20 °C

1.2: 0 °C

2.1: sodium tetrahydroborate; methanol / 2 h / 20 °C

3.1: sodium hydride / tetrahydrofuran / 0.33 h / Cooling with ice

3.2: 3 h / 20 °C

With hydrogenchloride; methanol; sodium tetrahydroborate; water; sodium hydride; In tetrahydrofuran;

Reference yield:

: 1224949-36-3
3-(8-hydroxy-1,4-dioxaspiro[4.5]decan-8-yl)-1-(p-tolyl)-2-propyn-1-one

: 1224949-11-4
4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl dimethylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / ethanol / 0.5 h / 20 °C

1.2: 15 h / 20 °C

2.1: hydrogenchloride; water / tetrahydrofuran / 15 h / 20 °C

2.2: 0 °C

3.1: sodium tetrahydroborate; methanol / 2 h / 20 °C

4.1: sodium hydride / tetrahydrofuran / 0.33 h / Cooling with ice

4.2: 3 h / 20 °C

With hydrogenchloride; methanol; sodium tetrahydroborate; water; sodium hydride; triethylamine; In tetrahydrofuran; ethanol;