3,4-Dimethoxy-benzoic acid 4-[(5,8-dimethoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-ethyl-amino]-butyl ester

Base Information

• Chemical Name: 3,4-Dimethoxy-benzoic acid 4-[(5,8-dimethoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-ethyl-amino]-butyl ester
• CAS No.: 82763-59-5
• Molecular Formula: C₂₇H₃₇NO₆
• Molecular Weight: 471.594

Synonyms:3,4-Dimethoxy-benzoic acid 4-[(5,8-dimethoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-ethyl-amino]-butyl ester

Chemical Property of 3,4-Dimethoxy-benzoic acid 4-[(5,8-dimethoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-ethyl-amino]-butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of 3,4-Dimethoxy-benzoic acid 4-[(5,8-dimethoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-ethyl-amino]-butyl ester

There total 3 articles about 3,4-Dimethoxy-benzoic acid 4-[(5,8-dimethoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-ethyl-amino]-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

SKF 88788 (81998-11-0) + 3,4-Dimethoxy-benzoic acid 4-chloro-butyl ester (69788-75-6) → 3,4-Dimethoxy-benzoic acid 4-[(5,8-dimethoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-ethyl-amino]-butyl ester (82763-59-5)

Guidance literature:

With sodium carbonate; sodium iodide; In butanone; for 96h; Heating;

DOI:10.1021/jm00353a016

Reference yield:

N-acetyl-5,8-dimethoxy-1,2,3,4-tetrahydro-2-naphthylamine (69788-89-2) → 3,4-Dimethoxy-benzoic acid 4-[(5,8-dimethoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-ethyl-amino]-butyl ester (82763-59-5)

Guidance literature:

Multi-step reaction with 2 steps

1: LiAlH₄ / tetrahydrofuran / 2.5 h / Heating

2: NaI, Na₂CO₃ / butan-2-one / 96 h / Heating

With lithium aluminium tetrahydride; sodium carbonate; sodium iodide; In tetrahydrofuran; butanone;

DOI:10.1021/jm00353a016

Reference yield:

→ 3,4-Dimethoxy-benzoic acid 4-[(5,8-dimethoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-ethyl-amino]-butyl ester (82763-59-5)

Guidance literature:

Entspr.Amin, Alkyl.;

upstream raw materials:

SKF 88788

3,4-Dimethoxy-benzoic acid 4-chloro-butyl ester

N-acetyl-5,8-dimethoxy-1,2,3,4-tetrahydro-2-naphthylamine

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