2-n-butyl-3-{4-[3-(di-n-butylamino)-propoxyl]-benzoyl}-5-bromo-benzofuran

Base Information

Chemical Name:2-n-butyl-3-{4-[3-(di-n-butylamino)-propoxyl]-benzoyl}-5-bromo-benzofuran
CAS No.:1338547-30-0
Molecular Formula:C₃₀H₄₀BrNO₃
Molecular Weight:542.557
Hs Code.:

Synonyms:2-n-butyl-3-{4-[3-(di-n-butylamino)-propoxyl]-benzoyl}-5-bromo-benzofuran

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Chemical Property of 2-n-butyl-3-{4-[3-(di-n-butylamino)-propoxyl]-benzoyl}-5-bromo-benzofuran

Chemical Property:

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Technology Process of 2-n-butyl-3-{4-[3-(di-n-butylamino)-propoxyl]-benzoyl}-5-bromo-benzofuran

There total 6 articles about 2-n-butyl-3-{4-[3-(di-n-butylamino)-propoxyl]-benzoyl}-5-bromo-benzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1338547-33-3
2-n-butyl-3-{4-[3-(di-n-butylamino)-propoxyl]-benzoyl}-5-bromo-benzofuran hydrochloride

: 1338547-30-0
2-n-butyl-3-{4-[3-(di-n-butylamino)-propoxyl]-benzoyl}-5-bromo-benzofuran

Guidance literature:: With potassium carbonate; In dichloromethane; water;

Reference yield: 67.0%

: 4-[3-(di-n-butylamino)-propoxy]-benzoic acid chloride hydrochloride

: 497225-66-8
2-n-butyl-5-bromo-benzofuran

: 1338547-30-0
2-n-butyl-3-{4-[3-(di-n-butylamino)-propoxyl]-benzoyl}-5-bromo-benzofuran

Guidance literature:: With aluminum (III) chloride; In dichloromethane; at 20 - 30 ℃; Inert atmosphere;

Reference yield:

: 1761-61-1
5-bromosalicyclaldehyde

: 1338547-30-0
2-n-butyl-3-{4-[3-(di-n-butylamino)-propoxyl]-benzoyl}-5-bromo-benzofuran

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 55 - 80 °C

1.2: 80 °C

2.1: sodium hydroxide; water / tert-butyl methyl ether / 20 - 40 °C

3.1: benzenesulfonyl chloride; triethylamine / toluene / 80 °C

4.1: aluminum (III) chloride / dichloromethane / 20 - 30 °C / Inert atmosphere

With aluminum (III) chloride; water; potassium carbonate; triethylamine; benzenesulfonyl chloride; sodium hydroxide; In dichloromethane; tert-butyl methyl ether; N,N-dimethyl-formamide; toluene;