(1S,2R,4R)-4-Benzyloxy-2-diphenylphosphinoyl-1-(4-methoxyphenyl)octyl acetate

Base Information

Chemical Name:(1S,2R,4R)-4-Benzyloxy-2-diphenylphosphinoyl-1-(4-methoxyphenyl)octyl acetate
CAS No.:245356-50-7
Molecular Formula:C₃₆H₄₁O₅P
Molecular Weight:584.692
Hs Code.:

Synonyms:(1S,2R,4R)-4-Benzyloxy-2-diphenylphosphinoyl-1-(4-methoxyphenyl)octyl acetate

Suppliers and Price of (1S,2R,4R)-4-Benzyloxy-2-diphenylphosphinoyl-1-(4-methoxyphenyl)octyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2R,4R)-4-Benzyloxy-2-diphenylphosphinoyl-1-(4-methoxyphenyl)octyl acetate

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Technology Process of (1S,2R,4R)-4-Benzyloxy-2-diphenylphosphinoyl-1-(4-methoxyphenyl)octyl acetate

There total 1 articles about (1S,2R,4R)-4-Benzyloxy-2-diphenylphosphinoyl-1-(4-methoxyphenyl)octyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 108-24-7
acetic anhydride

: 245356-49-4
(1S,2R,4R)-4-Benzyloxy-2-diphenylphosphinoyl-1-(4-methoxyphenyl)octan-1-ol

: 245356-50-7
(1S,2R,4R)-4-Benzyloxy-2-diphenylphosphinoyl-1-(4-methoxyphenyl)octyl acetate

Guidance literature:: In pyridine; for 48h;
DOI:10.1039/a903371h

Reference yield: 52.0%

: 245356-50-7
(1S,2R,4R)-4-Benzyloxy-2-diphenylphosphinoyl-1-(4-methoxyphenyl)octyl acetate

: (1S,2R,4R)-2-Diphenylphosphinoyl-4-hydroxy-1-(4-methoxyphenyl)octyl acetate

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 48h; under 3040 Torr;
DOI:10.1039/a903371h

Reference yield:

: 245356-50-7
(1S,2R,4R)-4-Benzyloxy-2-diphenylphosphinoyl-1-(4-methoxyphenyl)octyl acetate

: (1S,2R,3E)-2-Diphenylphosphinoyl-1-(4-methoxyphenyl)oct-3-enyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / H₂ / Pd/C / methanol / 48 h / 3040 Torr

2: 63 percent / PPh₃; DEAD; phthalimide / tetrahydrofuran / 16 h / 20 °C

With phthalimide; hydrogen; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In tetrahydrofuran; methanol; 1: Debenzylation / 2: Dehydration;
DOI:10.1039/a903371h