(3aR,8aS)-tert-butyl 3a-bromo-8a-phenyl-3,3a-dihydro-2H-furo[2,3-b]indole-8(8aH)-carboxylate

Base Information

• Chemical Name: (3aR,8aS)-tert-butyl 3a-bromo-8a-phenyl-3,3a-dihydro-2H-furo[2,3-b]indole-8(8aH)-carboxylate
• CAS No.: 1580471-44-8
• Molecular Formula: C₂₁H₂₂BrNO₃
• Molecular Weight: 416.315

Synonyms:(3aR,8aS)-tert-butyl 3a-bromo-8a-phenyl-3,3a-dihydro-2H-furo[2,3-b]indole-8(8aH)-carboxylate

Chemical Property of (3aR,8aS)-tert-butyl 3a-bromo-8a-phenyl-3,3a-dihydro-2H-furo[2,3-b]indole-8(8aH)-carboxylate

Chemical Property:

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Technology Process of (3aR,8aS)-tert-butyl 3a-bromo-8a-phenyl-3,3a-dihydro-2H-furo[2,3-b]indole-8(8aH)-carboxylate

There total 1 articles about (3aR,8aS)-tert-butyl 3a-bromo-8a-phenyl-3,3a-dihydro-2H-furo[2,3-b]indole-8(8aH)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl 3-(2-hydroxyethyl)-2-phenyl-1H-indole-1-carboxylate → (3aR,8aS)-tert-butyl 3a-bromo-8a-phenyl-3,3a-dihydro-2H-furo[2,3-b]indole-8(8aH)-carboxylate (1580471-44-8) + (3aS,8aR)-tert-butyl 3a-bromo-8a-phenyl-3,3a-dihydro-2H-furo[2,3-b]indole-8(8aH)-carboxylate

Guidance literature:

With C₁₅H₁₇F₆N₂⁽¹⁺⁾*Br₂*BF₄^(1-); 2C₁₅H₁₇F₆N₂⁽¹⁺⁾*3BF₄^(1-)*Br⁽¹⁺⁾; (R)-1,1'-binaphthyl-2,2'-phosphoric acid; sodium carbonate; In toluene; at 0 ℃; for 6.5h; Overall yield = 77 %; Overall yield = 32 mg; enantioselective reaction; Inert atmosphere; Enzymatic reaction;

DOI:10.1021/ol5004109

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