Technology Process of C37H47(2)H2N3O4
There total 6 articles about C37H47(2)H2N3O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
methanol;
at 50 ℃;
for 72h;
Inert atmosphere;
DOI:10.1002/anie.201200822
- Guidance literature:
-
Multi-step reaction with 8 steps
1: ethanol / 72 h / 20 °C / Inert atmosphere
2: sodium tetrahydroborate / ethanol / 24 h / 20 °C / Inert atmosphere
3: dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere
4: triethylamine / dichloromethane / 15 h / 20 °C / Inert atmosphere
5: sodium hydroxide / methanol; water / 5 h / 20 °C
6: ethanol / 72 h / 20 °C / Inert atmosphere
7: sodium borodeuteride / ethanol / 24 h / 20 °C / Inert atmosphere
8: N-ethyl-N,N-diisopropylamine / methanol / 72 h / 50 °C / Inert atmosphere
With
sodium tetrahydroborate; sodium borodeuteride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
methanol; ethanol; dichloromethane; water;
DOI:10.1002/anie.201200822
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium borodeuteride / ethanol / 24 h / 20 °C / Inert atmosphere
2: N-ethyl-N,N-diisopropylamine / methanol / 72 h / 50 °C / Inert atmosphere
With
sodium borodeuteride; N-ethyl-N,N-diisopropylamine;
In
methanol; ethanol;
DOI:10.1002/anie.201200822