3-(4-Nitro-benzoyl)-pyrrolo[2,1-a]isoquinoline-1,2-dicarboxylic acid diethyl ester

Base Information

• Chemical Name: 3-(4-Nitro-benzoyl)-pyrrolo[2,1-a]isoquinoline-1,2-dicarboxylic acid diethyl ester
• CAS No.: 84801-92-3
• Molecular Formula: C₂₅H₂₀N₂O₇
• Molecular Weight: 460.443

Synonyms:3-(4-Nitro-benzoyl)-pyrrolo[2,1-a]isoquinoline-1,2-dicarboxylic acid diethyl ester

Chemical Property of 3-(4-Nitro-benzoyl)-pyrrolo[2,1-a]isoquinoline-1,2-dicarboxylic acid diethyl ester

Chemical Property:

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Technology Process of 3-(4-Nitro-benzoyl)-pyrrolo[2,1-a]isoquinoline-1,2-dicarboxylic acid diethyl ester

There total 2 articles about 3-(4-Nitro-benzoyl)-pyrrolo[2,1-a]isoquinoline-1,2-dicarboxylic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

C17H13N2O3(1+)*I(1-) (6277-71-0) + acetylenedicarboxylic acid diethyl ester (762-21-0) → 3-(4-Nitro-benzoyl)-pyrrolo[2,1-a]isoquinoline-1,2-dicarboxylic acid diethyl ester (84801-92-3)

Guidance literature:

With iodine; In dimethyl sulfoxide; at 20 ℃; for 2h;

DOI:10.1007/s00706-013-1120-6

Reference yield: 50.0%

2-(2-(4-nitrophenyl)-2-oxoethyl)isoquinolin-2-ium bromide (39954-59-1) + acetylenedicarboxylic acid diethyl ester (762-21-0) → 3-(4-Nitro-benzoyl)-pyrrolo[2,1-a]isoquinoline-1,2-dicarboxylic acid diethyl ester (84801-92-3)

Guidance literature:

With triethylamine; In benzene; 1.) 1 h, 2.) reflux, 6 h;

DOI:10.1021/je00032a044

upstream raw materials:

2-(2-(4-nitrophenyl)-2-oxoethyl)isoquinolin-2-ium bromide

acetylenedicarboxylic acid diethyl ester

C₁₇H₁₃N₂O₃⁽¹⁺⁾*I^(1-)

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