7-Chlor-3-(2-chlorethyl)-2-oxo-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin

Base Information

Chemical Name:7-Chlor-3-(2-chlorethyl)-2-oxo-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin
CAS No.:99319-10-5
Molecular Formula:C₁₆H₁₃Cl₂N₃O
Molecular Weight:334.205
Hs Code.:

Synonyms:7-Chlor-3-(2-chlorethyl)-2-oxo-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin

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Chemical Property of 7-Chlor-3-(2-chlorethyl)-2-oxo-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin

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Technology Process of 7-Chlor-3-(2-chlorethyl)-2-oxo-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin

There total 3 articles about 7-Chlor-3-(2-chlorethyl)-2-oxo-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 86230-82-2
7-chloro-9-phenyl-1,2-dihydrooxazolo<2,3-b>-1,3,4-benzotriazepine

: 99319-10-5
7-Chlor-3-(2-chlorethyl)-2-oxo-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 1h;

Reference yield:

: 99319-11-6
7-Chlor-3-(2-hydroxyethyl)-2-oxo-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin

: 99319-10-5
7-Chlor-3-(2-chlorethyl)-2-oxo-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin

Guidance literature:: With hydrogenchloride;

Reference yield:

: 99319-09-2
3-(2-Bromethyl)-7-chlor-2-oxo-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin

: 99319-10-5
7-Chlor-3-(2-chlorethyl)-2-oxo-5-phenyl-1,2-dihydro-3H-1,3,4-benzotriazepin

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine

2: 60 percent / 36percent HCl / dioxane / 1 h / 20 °C

With piperidine; hydrogenchloride; In 1,4-dioxane;