N-benzyloxycarbonyl-D-glutamyl α-benzyl ester γ--L-lysine t-butyl ester

Base Information

Chemical Name:N-benzyloxycarbonyl-D-glutamyl α-benzyl ester γ--L-lysine t-butyl ester
CAS No.:87796-95-0
Molecular Formula:C₃₈H₄₇N₃O₉
Molecular Weight:689.806
Hs Code.:

N-benzyloxycarbonyl-D-glutamyl α-benzyl ester γ-<N(ε)-benzyloxycarbonyl>-L-lysine t-butyl ester

Synonyms:N-benzyloxycarbonyl-D-glutamyl α-benzyl ester γ--L-lysine t-butyl ester

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Chemical Property of N-benzyloxycarbonyl-D-glutamyl α-benzyl ester γ--L-lysine t-butyl ester

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Technology Process of N-benzyloxycarbonyl-D-glutamyl α-benzyl ester γ--L-lysine t-butyl ester

There total 1 articles about N-benzyloxycarbonyl-D-glutamyl α-benzyl ester γ--L-lysine t-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 5978-22-3,1426213-63-9
N(ε)-benzoyloxycarbonyl-L-lysine tert-butyl ester hydrochloride

: N-benzyloxycarbonyl-D-glutamic acid α-benzyl ester dicyclohexylammonium salt

: 87796-95-0
N-benzyloxycarbonyl-D-glutamyl α-benzyl ester γ--L-lysine t-butyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; for 21h; Ambient temperature;

Reference yield: 85.0%

: 87796-95-0
N-benzyloxycarbonyl-D-glutamyl α-benzyl ester γ--L-lysine t-butyl ester

: 87796-96-1
N-benzyloxycarbonyl-D-glutamyl α-benzyl ester γ--L-lysine

Guidance literature:: With water; In trifluoroacetic acid; for 0.5h; Ambient temperature;

Reference yield:

: 87796-95-0
N-benzyloxycarbonyl-D-glutamyl α-benzyl ester γ--L-lysine t-butyl ester

: N-benzyloxycarbonyl-D-glutamyl α-benzyl ester γ--L-lysyl-6-aminopenicillanic acid 4-nitrobenzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / H₂O / trifluoroacetic acid / 0.5 h / Ambient temperature

2: 0.73 g / Et₃N, 1-hydroxybenzotriazole monohydrate, N,N'-dicyclohexylcarbodiimide / CH₂Cl₂ / 16 h / 0 °C

With water; 1-hydroxybenzotriazol-hydrate; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; trifluoroacetic acid;