Di(3-methyl phenyl)sulfone

Base Information

Chemical Name:Di(3-methyl phenyl)sulfone
CAS No.:5097-13-2
Molecular Formula:C₁₄H₁₄O₂S
Molecular Weight:246.33
Hs Code.:
DSSTox Substance ID:DTXSID101337837
Nikkaji Number:J677.589F

Synonyms:di(3-methyl phenyl)sulfone;SCHEMBL822302;NZOSGGNRVDMIHW-UHFFFAOYSA-N;DTXSID101337837;1,1'-Sulfonylbis[3-methylbenzene];5097-13-2

Suppliers and Price of Di(3-methyl phenyl)sulfone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of Di(3-methyl phenyl)sulfone

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:246.07145086
Heavy Atom Count:17
Complexity:314

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC(=CC=C1)S(=O)(=O)C2=CC=CC(=C2)C

Technology Process of Di(3-methyl phenyl)sulfone

There total 13 articles about Di(3-methyl phenyl)sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 591-17-3
meta-bromotoluene

: 5097-13-2
3,3'-sulfonylbis(methylbenzene)

Guidance literature:: meta-bromotoluene; With tert.-butyl lithium; In n-heptane; dibutyl ether; at -10 - 20 ℃; Inert atmosphere; Schlenk technique;

With 1,4-diazabicyclo [2.2.2] octane-1,4-diium-1,4-disulfinate; In 1,4-dioxane; n-heptane; dibutyl ether; at 20 ℃; for 2h; Inert atmosphere; Schlenk technique;

meta-bromotoluene; With palladium diacetate; caesium carbonate; (9,9-dimethyl-9H-xanthene-4,5-diyl)bis(bis(3,5-bis(trifluoromethyl)phenyl)phosphine); In 1,4-dioxane; n-heptane; dibutyl ether; at 110 ℃; for 16h; Inert atmosphere; Schlenk technique; Sealed tube;
DOI:10.1002/anie.201305369

Reference yield: 95.0%

: 5097-13-2
3,3'-sulfonylbis(methylbenzene)

Guidance literature:: With 2C₂H₃O₂^(1-)*C₂₆H₃₀B₁₀P₂*Cu⁽²⁺⁾; In toluene; at 20 ℃; for 3h;

Reference yield: 91.0%

: 1073-06-9
3-fluorobromobenzene

: 591-17-3
meta-bromotoluene

: 1-fluoro-3-(m-tolylsulfonyl)benzene

: 5097-13-2
3,3'-sulfonylbis(methylbenzene)

Guidance literature:: meta-bromotoluene; With tert.-butyl lithium; In n-heptane; dibutyl ether; at -10 - 20 ℃; Inert atmosphere; Schlenk technique;

With 1,4-diazabicyclo [2.2.2] octane-1,4-diium-1,4-disulfinate; In 1,4-dioxane; n-heptane; dibutyl ether; at 20 ℃; for 2h; Inert atmosphere; Schlenk technique;

3-fluorobromobenzene; With palladium diacetate; caesium carbonate; (9,9-dimethyl-9H-xanthene-4,5-diyl)bis(bis(3,5-bis(trifluoromethyl)phenyl)phosphine); In 1,4-dioxane; n-heptane; dibutyl ether; at 110 ℃; for 16h; Inert atmosphere; Schlenk technique; Sealed tube;
DOI:10.1002/anie.201305369