1-deoxy-2,3:4,5-di-O-isopropylidene-1-{4-[(phenylmethyl)amino]phenyl}-D-ribitol

Base Information

• Chemical Name: 1-deoxy-2,3:4,5-di-O-isopropylidene-1-{4-[(phenylmethyl)amino]phenyl}-D-ribitol
• CAS No.: 1000163-01-8
• Molecular Formula: C₂₄H₃₁NO₄
• Molecular Weight: 397.514

Synonyms:1-deoxy-2,3:4,5-di-O-isopropylidene-1-{4-[(phenylmethyl)amino]phenyl}-D-ribitol

Chemical Property of 1-deoxy-2,3:4,5-di-O-isopropylidene-1-{4-[(phenylmethyl)amino]phenyl}-D-ribitol

Chemical Property:

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Technology Process of 1-deoxy-2,3:4,5-di-O-isopropylidene-1-{4-[(phenylmethyl)amino]phenyl}-D-ribitol

There total 1 articles about 1-deoxy-2,3:4,5-di-O-isopropylidene-1-{4-[(phenylmethyl)amino]phenyl}-D-ribitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

N-{4-[(1S)-2,3:4,5-di-O-isopropylidene-D-ribitol-1-C-yl]phenyl}benzenamide → 1-deoxy-2,3:4,5-di-O-isopropylidene-1-{4-[(phenylmethyl)amino]phenyl}-D-ribitol (1000163-01-8)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 80 ℃; for 30h;

DOI:10.1002/hlca.200790195

Reference yield: 90.0%

1-deoxy-2,3:4,5-di-O-isopropylidene-1-{4-[(phenylmethyl)amino]phenyl}-D-ribitol (1000163-01-8) → 1-(4-aminophenyl)-1-deoxy-2,3:4,5-di-O-isopropylidene-D-ribitol (173932-50-8)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol;

DOI:10.1002/hlca.200790195

Reference yield: 83.0%

1-deoxy-2,3:4,5-di-O-isopropylidene-1-{4-[(phenylmethyl)amino]phenyl}-D-ribitol (1000163-01-8) → 1-deoxy-1-{4-[(phenylmethyl)amino]phenyl}-D-ribitol

Guidance literature:

With hydrogenchloride; at 100 ℃; for 1h;

DOI:10.1002/hlca.200790195

Downstream raw materials:

1-(4-aminophenyl)-1-deoxy-2,3:4,5-di-O-isopropylidene-D-ribitol

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