N-methyl-(Z)-4'-benzoyloxy-2'-butenyl but-2-ynamide

Base Information

Chemical Name:N-methyl-(Z)-4'-benzoyloxy-2'-butenyl but-2-ynamide
CAS No.:891847-07-7
Molecular Formula:C₁₆H₁₇NO₃
Molecular Weight:271.316
Hs Code.:

Synonyms:N-methyl-(Z)-4'-benzoyloxy-2'-butenyl but-2-ynamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methyl-(Z)-4'-benzoyloxy-2'-butenyl but-2-ynamide

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Technology Process of N-methyl-(Z)-4'-benzoyloxy-2'-butenyl but-2-ynamide

There total 2 articles about N-methyl-(Z)-4'-benzoyloxy-2'-butenyl but-2-ynamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 892848-68-9
4-methylamino-but-2-enyl benzoate

: 590-93-2
2-Butynoic acid

: 891847-07-7
N-methyl-(Z)-4'-benzoyloxy-2'-butenyl but-2-ynamide

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at -20 - 20 ℃;
DOI:10.1021/jo050121n

Reference yield:

: 116664-13-2
(Z)-4-(benzoyloxy)-1-bromobut-2-ene

: 891847-07-7
N-methyl-(Z)-4'-benzoyloxy-2'-butenyl but-2-ynamide

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / CH₂Cl₂; ethanol / 0.5 h / 20 °C

2: 60 percent / 1,3-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / CH₂Cl₂ / -20 - 20 °C

With dmap; dicyclohexyl-carbodiimide; In ethanol; dichloromethane;
DOI:10.1021/jo050121n