2-Azetidinone,3-amino-4-[[(tetrahydro-2H-pyran-2-yl)oxy]methyl]-,[3alpha,4alpha(S*)]-(9CI)

Base Information

Chemical Name:2-Azetidinone,3-amino-4-[[(tetrahydro-2H-pyran-2-yl)oxy]methyl]-,[3alpha,4alpha(S*)]-(9CI)
CAS No.:766468-92-2
Molecular Formula:C₉H₁₆N₂O₃
Molecular Weight:200.238
Hs Code.:
Mol file:766468-92-2.mol

Synonyms:2-Azetidinone,3-amino-4-[[(tetrahydro-2H-pyran-2-yl)oxy]methyl]-, [3a,4a(S*)]- (9CI)

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Chemical Property of 2-Azetidinone,3-amino-4-[[(tetrahydro-2H-pyran-2-yl)oxy]methyl]-,[3alpha,4alpha(S*)]-(9CI)

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Technology Process of 2-Azetidinone,3-amino-4-[[(tetrahydro-2H-pyran-2-yl)oxy]methyl]-,[3alpha,4alpha(S*)]-(9CI)

There total 2 articles about 2-Azetidinone,3-amino-4-[[(tetrahydro-2H-pyran-2-yl)oxy]methyl]-,[3alpha,4alpha(S*)]-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107699-64-9,107795-34-6
(3RS,4RS) 3-(<(phenylmethyl)-oxy>-carbonyl)-amino 4-(<(tetrahydropyran-2-yl)-oxy>-methyl) azetidin-2-one

: 766468-92-2,781574-86-5
(3RS,4RS) 3-amino 4(<(tetrahydropyran-2-yl)-oxy>-methyl) azetidin-2-one

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; at 20 ℃; for 0.25h; Yield given;
DOI:10.1016/S0040-4020(01)90553-8

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 766468-92-2,781574-86-5
(3RS,4RS) 3-amino 4(<(tetrahydropyran-2-yl)-oxy>-methyl) azetidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / p-toluenesulfonic acid / tetrahydrofuran / 20 h / 20 °C

2: hydrogen / 5percent Pd/C / ethanol / 0.25 h / 20 °C

With hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1016/S0040-4020(01)90553-8