4-(Dimethylamino)-4-phenyl-1-thia-3-azoniabutatriene Hexachloroantimonate

Base Information

• Chemical Name: 4-(Dimethylamino)-4-phenyl-1-thia-3-azoniabutatriene Hexachloroantimonate
• CAS No.: 113290-08-7
• Molecular Formula: C₁₀H₁₁N₂S*Cl₆Sb
• Molecular Weight: 525.745

Synonyms:4-(Dimethylamino)-4-phenyl-1-thia-3-azoniabutatriene Hexachloroantimonate

Chemical Property of 4-(Dimethylamino)-4-phenyl-1-thia-3-azoniabutatriene Hexachloroantimonate

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Technology Process of 4-(Dimethylamino)-4-phenyl-1-thia-3-azoniabutatriene Hexachloroantimonate

There total 1 articles about 4-(Dimethylamino)-4-phenyl-1-thia-3-azoniabutatriene Hexachloroantimonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

(chlorophenylmethylene)(dimethylammonium) hexachloroantimonate (110090-12-5) + ammonium thiocyanate (1147550-11-5) → 4-(Dimethylamino)-4-phenyl-1-thia-3-azoniabutatriene Hexachloroantimonate (113290-08-7)

Guidance literature:

In dichloromethane; at 23 ℃; for 48h;

Reference yield: 88.0%

4-(Dimethylamino)-4-phenyl-1-thia-3-azoniabutatriene Hexachloroantimonate (113290-08-7) + benzylidene phenylamine (538-51-2) → N2-(3,4-Diphenyl-1,3-thiazetidin-2-ylidene)-N1,N1-dimethylbenzamidinium Hexachloroantimonate (123438-85-7)

Guidance literature:

In dichloromethane; for 0.25h; Ambient temperature;

Reference yield: 84.0%

N-(n-Butyl)diphenylketene imine (21843-89-0) + 4-(Dimethylamino)-4-phenyl-1-thia-3-azoniabutatriene Hexachloroantimonate (113290-08-7) → N2-<3-Butyl-4-(diphenylmethylene)-1,3-thiazetidin-2-ylidene>-N1,N1-dimethylbenzamidinium Hexachloroantimonate (123439-03-2)

Guidance literature:

In dichloromethane; at 0 ℃; for 0.25h;

upstream raw materials:

(chlorophenylmethylene)(dimethylammonium) hexachloroantimonate

ammonium thiocyanate

Downstream raw materials:

N²-(3-Isopropyl-4-phenyl-1,3-thiazetidin-2-ylidene)-N¹,N¹-dimethylbenzamidinium Hexachloroantimonate

N²-(3-tert-Butyl-4-phenyl-1,3-thiazetidin-2-ylidene)-N¹,N¹-dimethylbenzamidinium Hexachloroantimonate

N²-<3-Butyl-4-(diphenylmethylene)-1,3-thiazetidin-2-ylidene>-N¹,N¹-dimethylbenzamidinium Hexachloroantimonate

N²-<3-<4-(Dimethylamino)phenyl>-4-<4-(dimethylamino)phenylimino>-1,3-thiazetidin-2-ylidene>-N¹,N¹-dimethylbenzamidinium Hexachloroantimonate

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