C₃₀H₃₉BrN₄O₄

Base Information

• Chemical Name: C₃₀H₃₉BrN₄O₄
• CAS No.: 1327337-03-0
• Molecular Formula: C₃₀H₃₉BrN₄O₄
• Molecular Weight: 599.568
• Mol file: 1327337-03-0.mol

Synonyms:C₃₀H₃₉BrN₄O₄

Chemical Property of C₃₀H₃₉BrN₄O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₃₉BrN₄O₄

There total 6 articles about C₃₀H₃₉BrN₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C22H23BrN2O (1301177-23-0) → C30H39BrN4O4 (1327337-03-0)

Guidance literature:

Multi-step reaction with 6 steps

1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tert-butyl alcohol

2: sodium periodate; silica gel / dichloromethane

3: sodium tetrahydroborate / tetrahydrofuran / 0 °C

4: triethylamine / dichloromethane

6: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

With sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; silica gel; benzotriazol-1-ol; 4-methylmorpholine N-oxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane; tert-butyl alcohol;

DOI:10.1016/j.bmcl.2011.03.112

Reference yield:

C22H25BrN2O3 (1301177-25-2) → C30H39BrN4O4 (1327337-03-0)

Guidance literature:

Multi-step reaction with 5 steps

1: sodium periodate; silica gel / dichloromethane

2: sodium tetrahydroborate / tetrahydrofuran / 0 °C

3: triethylamine / dichloromethane

5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

With sodium tetrahydroborate; sodium periodate; silica gel; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1016/j.bmcl.2011.03.112

Reference yield:

C21H21BrN2O2 (1301177-27-4) → C30H39BrN4O4 (1327337-03-0)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium tetrahydroborate / tetrahydrofuran / 0 °C

2: triethylamine / dichloromethane

4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

With sodium tetrahydroborate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1016/j.bmcl.2011.03.112

upstream raw materials:

C₂₂H₂₃BrN₂O

C₂₂H₂₅BrN₂O₃

C₂₁H₂₁BrN₂O₂

L-N-Boc-Ala

Downstream raw materials:

C₂₅H₃₁BrN₄O₂