methyl N-(N-tert-butoxycarbonyl-L-seryl)-S-[6-nitro-2-carboxylbenzyl]-L-cysteinate

Base Information

Chemical Name:methyl N-(N-tert-butoxycarbonyl-L-seryl)-S-[6-nitro-2-carboxylbenzyl]-L-cysteinate
CAS No.:676347-17-4
Molecular Formula:C₂₀H₂₇N₃O₁₀S
Molecular Weight:501.514
Hs Code.:

Synonyms:methyl N-(N-tert-butoxycarbonyl-L-seryl)-S-[6-nitro-2-carboxylbenzyl]-L-cysteinate

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Chemical Property of methyl N-(N-tert-butoxycarbonyl-L-seryl)-S-[6-nitro-2-carboxylbenzyl]-L-cysteinate

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Technology Process of methyl N-(N-tert-butoxycarbonyl-L-seryl)-S-[6-nitro-2-carboxylbenzyl]-L-cysteinate

There total 4 articles about methyl N-(N-tert-butoxycarbonyl-L-seryl)-S-[6-nitro-2-carboxylbenzyl]-L-cysteinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 0.69%

: C₂₆H₄₁N₃O₁₀SSi

: 676347-17-4
methyl N-(N-tert-butoxycarbonyl-L-seryl)-S-[6-nitro-2-carboxylbenzyl]-L-cysteinate

Guidance literature:: With ammonium fluoride; In methanol; at 20 ℃; for 0.5h;
DOI:10.1021/jm0310232

Reference yield:

: 1975-50-4
2-methyl-3-nitrobenzic acid

: 676347-17-4
methyl N-(N-tert-butoxycarbonyl-L-seryl)-S-[6-nitro-2-carboxylbenzyl]-L-cysteinate

Guidance literature:: Multi-step reaction with 4 steps

1: 55 percent / Et₃N / dimethylformamide / 24 h / 20 °C

2: 74 percent / NBS / CCl₄ / 0.67 h / 90 °C / Irradiation

3: Et₃N / CH₂Cl₂ / 2 h / 0 - 20 °C

4: 0.69 percent / NH₄F / methanol / 0.5 h / 20 °C

With ammonium fluoride; N-Bromosuccinimide; triethylamine; In methanol; tetrachloromethane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm0310232

Reference yield:

: 676347-14-1
(tert-butyl)dimethylsilyl 3-nitro-2-methylbenzoate

: 676347-17-4
methyl N-(N-tert-butoxycarbonyl-L-seryl)-S-[6-nitro-2-carboxylbenzyl]-L-cysteinate

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / NBS / CCl₄ / 0.67 h / 90 °C / Irradiation

2: Et₃N / CH₂Cl₂ / 2 h / 0 - 20 °C

3: 0.69 percent / NH₄F / methanol / 0.5 h / 20 °C

With ammonium fluoride; N-Bromosuccinimide; triethylamine; In methanol; tetrachloromethane; dichloromethane;
DOI:10.1021/jm0310232