6-C-phenyl-5-azido-3,5,6-trideoxy-1,2-O-isopropylidene-β-L-talofuranose

Base Information

Chemical Name:6-C-phenyl-5-azido-3,5,6-trideoxy-1,2-O-isopropylidene-β-L-talofuranose
CAS No.:131013-19-9
Molecular Formula:C₁₅H₁₉N₃O₃
Molecular Weight:289.334
Hs Code.:

Synonyms:6-C-phenyl-5-azido-3,5,6-trideoxy-1,2-O-isopropylidene-β-L-talofuranose

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Chemical Property of 6-C-phenyl-5-azido-3,5,6-trideoxy-1,2-O-isopropylidene-β-L-talofuranose

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Technology Process of 6-C-phenyl-5-azido-3,5,6-trideoxy-1,2-O-isopropylidene-β-L-talofuranose

There total 4 articles about 6-C-phenyl-5-azido-3,5,6-trideoxy-1,2-O-isopropylidene-β-L-talofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 131013-18-8
6-C-phenyl-3,6-dideoxy-5-O-(p-tolylsulfonyl)-1,2-O-isopropylidene-α-D-allofuranose

: 131013-20-2
(3aR,5S,6aR)-2,2-Dimethyl-5-((E)-styryl)-tetrahydro-furo[2,3-d][1,3]dioxole

: 131013-19-9
6-C-phenyl-5-azido-3,5,6-trideoxy-1,2-O-isopropylidene-β-L-talofuranose

Guidance literature:: With sodium azide; In dimethyl sulfoxide; at 80 ℃; for 3h;
DOI:10.1021/jo00003a040

Reference yield:

: 2457-93-4
(3aR,5S,6aR)-2,2-dimethyl-5-[(2R)-oxiran-2-yl]-3a,5,6,6a-tetrahydrofuro[2,3-d] [1,3]dioxole

: 131013-19-9
6-C-phenyl-5-azido-3,5,6-trideoxy-1,2-O-isopropylidene-β-L-talofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / CuI / tetrahydrofuran / a) 1 h at -50 deg C and 30 min at -30 deg C

2: 95 percent / pyridine / 24 h / 45 °C

3: 90 percent / NaN₃ / dimethylsulfoxide / 3 h / 80 °C

With pyridine; copper(l) iodide; sodium azide; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1021/jo00003a040

Reference yield:

: 131013-17-7
6-C-phenyl-3,6-dideoxy-1,2-O-isopropylidene-α-D-allofuranose

: 131013-19-9
6-C-phenyl-5-azido-3,5,6-trideoxy-1,2-O-isopropylidene-β-L-talofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / pyridine / 24 h / 45 °C

2: 90 percent / NaN₃ / dimethylsulfoxide / 3 h / 80 °C

With pyridine; sodium azide; In dimethyl sulfoxide;
DOI:10.1021/jo00003a040