p-methoxyphenyl 2-O-allyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

Base Information

Chemical Name:p-methoxyphenyl 2-O-allyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside
CAS No.:1622258-17-6
Molecular Formula:C₃₀H₃₂O₇
Molecular Weight:504.58
Hs Code.:

Synonyms:p-methoxyphenyl 2-O-allyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-methoxyphenyl 2-O-allyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

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Technology Process of p-methoxyphenyl 2-O-allyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

There total 4 articles about p-methoxyphenyl 2-O-allyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 106-95-6
allyl bromide

: 303127-81-3
p-methoxyphenyl 3-O-benzyl-4,6-di-O-benzylidene-β-D-glucopyranoside

: 1622258-17-6
p-methoxyphenyl 2-O-allyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 4h; Inert atmosphere; Schlenk technique;
DOI:10.1002/ejoc.201402260

Reference yield:

: 3150-20-7,6032-32-2,28541-75-5,85481-53-4,89731-58-8,109121-56-4,121468-39-1,12167-34-9
4-methoxyphenyl β-D-glucopyranoside

: 1622258-17-6
p-methoxyphenyl 2-O-allyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: camphorsulfonic acid / N,N-dimethyl-formamide / 8 h / 60 °C / 180.02 Torr / Inert atmosphere; Schlenk technique

2.1: di(n-butyl)tin oxide / methanol / 24 h / Inert atmosphere; Schlenk technique; Reflux

2.2: 72 h / 20 °C / Inert atmosphere; Schlenk technique

3.1: sodium hydride / N,N-dimethyl-formamide / 4 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

With sodium hydride; di(n-butyl)tin oxide; In methanol; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201402260

Reference yield:

: 4-methoxyphenyl 4,6-di-O-benzylidene-β-D-glucopyranoside

: 1622258-17-6
p-methoxyphenyl 2-O-allyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: di(n-butyl)tin oxide / methanol / 24 h / Inert atmosphere; Schlenk technique; Reflux

1.2: 72 h / 20 °C / Inert atmosphere; Schlenk technique

2.1: sodium hydride / N,N-dimethyl-formamide / 4 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

With sodium hydride; di(n-butyl)tin oxide; In methanol; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201402260