(2R,3S,4S,5R)-3,4,5-tris(benzyloxy)-2-<(benzyloxy)methyl>-6-ethoxy-2,3,4,5-tetrahydropyridine

Base Information

• Chemical Name: (2R,3S,4S,5R)-3,4,5-tris(benzyloxy)-2-<(benzyloxy)methyl>-6-ethoxy-2,3,4,5-tetrahydropyridine
• CAS No.: 153996-65-7
• Molecular Formula: C₃₆H₃₉NO₅
• Molecular Weight: 565.709

Synonyms:(2R,3S,4S,5R)-3,4,5-tris(benzyloxy)-2-<(benzyloxy)methyl>-6-ethoxy-2,3,4,5-tetrahydropyridine

Chemical Property of (2R,3S,4S,5R)-3,4,5-tris(benzyloxy)-2-<(benzyloxy)methyl>-6-ethoxy-2,3,4,5-tetrahydropyridine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2R,3S,4S,5R)-3,4,5-tris(benzyloxy)-2-<(benzyloxy)methyl>-6-ethoxy-2,3,4,5-tetrahydropyridine

There total 1 articles about (2R,3S,4S,5R)-3,4,5-tris(benzyloxy)-2-<(benzyloxy)methyl>-6-ethoxy-2,3,4,5-tetrahydropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

triethyloxonium fluoroborate (368-39-8) + (3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)piperidin-2-one (77174-08-4) → (2R,3S,4S,5R)-3,4,5-tris(benzyloxy)-2-<(benzyloxy)methyl>-6-ethoxy-2,3,4,5-tetrahydropyridine (153996-65-7)

Guidance literature:

With triethylamine; In dichloromethane; 1.) RT, 26 h; 2.) RT, 1 h;

DOI:10.1002/hlca.19930760723

Reference yield: 86.0%

(2R,3S,4S,5R)-3,4,5-tris(benzyloxy)-2-<(benzyloxy)methyl>-6-ethoxy-2,3,4,5-tetrahydropyridine (153996-65-7) → 2,3,4,6-tetra-O-benzyl-D-glucon(15N)hydroximo-1,5-lactam

Guidance literature:

With [¹⁵N]hydroxylamine hydrochloride; sodium hydrogencarbonate; In methanol;

DOI:10.1002/hlca.19930760723

Reference yield: 31.0%

(2R,3S,4S,5R)-3,4,5-tris(benzyloxy)-2-<(benzyloxy)methyl>-6-ethoxy-2,3,4,5-tetrahydropyridine (153996-65-7) → (3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)piperidin-2-one (77174-08-4) + 2,3,4,6-tetra-O-benzyl-D-gluconhydroximo-1,5-lactam (153996-66-8)

Guidance literature:

With molecular sieve; hydroxylamine; In methanol; for 0.666667h; Ambient temperature;

DOI:10.1002/hlca.19930760723

upstream raw materials:

triethyloxonium fluoroborate

(3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)piperidin-2-one

Downstream raw materials:

(3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)piperidin-2-one

2,3,4,6-tetra-O-benzyl-D-gluconhydroximo-1,5-lactam

2,3,4,6-tetra-O-benzyl-D-mannothiolactam

2,3,4,6-tetra-O-benzyl-D-glucono-δ-thiolactam

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 153996-65-7 (2R,3S,4S,5R)-3,4,5-tris(benzyloxy)-2-<(benzyloxy)methyl>-6-ethoxy-2,3,4,5-tetrahydropyridine

Send

Send

Metric Ton KG G Pound L ML

Send

Send