2,9-Bis-bromomethyl-4-p-tolyl-[1,10]phenanthroline

Base Information

Chemical Name:2,9-Bis-bromomethyl-4-p-tolyl-[1,10]phenanthroline
CAS No.:181281-07-2
Molecular Formula:C₂₁H₁₆Br₂N₂
Molecular Weight:456.179
Hs Code.:

Synonyms:2,9-Bis-bromomethyl-4-p-tolyl-[1,10]phenanthroline

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Chemical Property of 2,9-Bis-bromomethyl-4-p-tolyl-[1,10]phenanthroline

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Technology Process of 2,9-Bis-bromomethyl-4-p-tolyl-[1,10]phenanthroline

There total 8 articles about 2,9-Bis-bromomethyl-4-p-tolyl-[1,10]phenanthroline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18978-78-4
2-methyl-8-aminoquinoline

: 181281-07-2
2,9-Bis-bromomethyl-4-p-tolyl-[1,10]phenanthroline

Guidance literature:: Multi-step reaction with 7 steps

1: 81 percent / conc. HCl, KH₂AsO₃ / 7 h / 80 °C

2: 73 percent / N-chlorosuccinimide, 3-chloroperoxybenzoic acid / CHCl₃; CCl₄ / 12 h / Heating

3: 67 percent / aq. formic acid / 40 h / Heating

4: thionyl chloride / 1 h / Heating

5: 0.5 h / Heating

6: NaBH₄ / ethanol / 3 h / Heating

7: 49percent aq. HBr / 3 h / Heating

With hydrogenchloride; sodium tetrahydroborate; N-chloro-succinimide; formic acid; thionyl chloride; potassium hydrogen arsenite; hydrogen bromide; 3-chloro-benzenecarboperoxoic acid; In tetrachloromethane; ethanol; chloroform;

Reference yield:

: 3837-95-4
(E)-1-(4-methylphenyl)-2-buten-1-one

: 181281-07-2
2,9-Bis-bromomethyl-4-p-tolyl-[1,10]phenanthroline

Guidance literature:: Multi-step reaction with 7 steps

1: 81 percent / conc. HCl, KH₂AsO₃ / 7 h / 80 °C

2: 73 percent / N-chlorosuccinimide, 3-chloroperoxybenzoic acid / CHCl₃; CCl₄ / 12 h / Heating

3: 67 percent / aq. formic acid / 40 h / Heating

4: thionyl chloride / 1 h / Heating

5: 0.5 h / Heating

6: NaBH₄ / ethanol / 3 h / Heating

7: 49percent aq. HBr / 3 h / Heating

With hydrogenchloride; sodium tetrahydroborate; N-chloro-succinimide; formic acid; thionyl chloride; potassium hydrogen arsenite; hydrogen bromide; 3-chloro-benzenecarboperoxoic acid; In tetrachloromethane; ethanol; chloroform;

Reference yield:

: 181281-02-7
4-(4-methylphenyl)-2,9-dimethyl-1,10-phenanthroline

: 181281-07-2
2,9-Bis-bromomethyl-4-p-tolyl-[1,10]phenanthroline

Guidance literature:: Multi-step reaction with 6 steps

1: 73 percent / N-chlorosuccinimide, 3-chloroperoxybenzoic acid / CHCl₃; CCl₄ / 12 h / Heating

2: 67 percent / aq. formic acid / 40 h / Heating

3: thionyl chloride / 1 h / Heating

4: 0.5 h / Heating

5: NaBH₄ / ethanol / 3 h / Heating

6: 49percent aq. HBr / 3 h / Heating

With sodium tetrahydroborate; N-chloro-succinimide; formic acid; thionyl chloride; hydrogen bromide; 3-chloro-benzenecarboperoxoic acid; In tetrachloromethane; ethanol; chloroform;