2-bromo-4-n-pentylbenzyl alcohol

Base Information

Chemical Name:2-bromo-4-n-pentylbenzyl alcohol
CAS No.:186962-76-5
Molecular Formula:C₁₂H₁₇BrO
Molecular Weight:257.17
Hs Code.:

Synonyms:2-bromo-4-n-pentylbenzyl alcohol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-bromo-4-n-pentylbenzyl alcohol

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Technology Process of 2-bromo-4-n-pentylbenzyl alcohol

There total 5 articles about 2-bromo-4-n-pentylbenzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 186962-74-3
2-bromo-4-n-pentylbenzoic acid

: 186962-76-5
2-bromo-4-n-pentylbenzyl alcohol

Guidance literature:: With borane; In tetrahydrofuran; for 4h; Heating;
DOI:10.1021/ja9638418

Reference yield:

: 79568-30-2
4,4-dimethyl-2-p-tolyl-2-oxazoline

: 186962-76-5
2-bromo-4-n-pentylbenzyl alcohol

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) diisopropylamine, n-BuLi / 1) THF, hexane, 0-5 deg C, 30 min; 2) THF, hexane, 0 deg C --> rt

2: 1.) n-BuLi, 2.) Br₂ / 1) THF, hexane, -45 deg C, 2 h; 2) THF, hexane, rt, overnight

3: 1.) aq. HCl, 2.) NaOH / 1) reflux, 1 h; 2) MeOH, H₂O

4: 82 percent / borane / tetrahydrofuran / 4 h / Heating

With hydrogenchloride; sodium hydroxide; n-butyllithium; borane; bromine; diisopropylamine; In tetrahydrofuran;
DOI:10.1021/ja9638418

Reference yield:

: 874-60-2
4-methyl-benzoyl chloride

: 186962-76-5
2-bromo-4-n-pentylbenzyl alcohol

Guidance literature:: Multi-step reaction with 5 steps

1: 78 percent / thionyl chloride

2: 1.) diisopropylamine, n-BuLi / 1) THF, hexane, 0-5 deg C, 30 min; 2) THF, hexane, 0 deg C --> rt

3: 1.) n-BuLi, 2.) Br₂ / 1) THF, hexane, -45 deg C, 2 h; 2) THF, hexane, rt, overnight

4: 1.) aq. HCl, 2.) NaOH / 1) reflux, 1 h; 2) MeOH, H₂O

5: 82 percent / borane / tetrahydrofuran / 4 h / Heating

With hydrogenchloride; sodium hydroxide; n-butyllithium; thionyl chloride; borane; bromine; diisopropylamine; In tetrahydrofuran;
DOI:10.1021/ja9638418