(±)-N-(1-(4-chlorophenyl)but-3-enyloxy)-2-(trimethylsilyl)-ethanesulfonamide

Base Information

• Chemical Name: (±)-N-(1-(4-chlorophenyl)but-3-enyloxy)-2-(trimethylsilyl)-ethanesulfonamide
• CAS No.: 1393744-91-6
• Molecular Formula: C₁₅H₂₄ClNO₃SSi
• Molecular Weight: 361.965

Synonyms:(±)-N-(1-(4-chlorophenyl)but-3-enyloxy)-2-(trimethylsilyl)-ethanesulfonamide

Chemical Property of (±)-N-(1-(4-chlorophenyl)but-3-enyloxy)-2-(trimethylsilyl)-ethanesulfonamide

Chemical Property:

Purity/Quality:

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Technology Process of (±)-N-(1-(4-chlorophenyl)but-3-enyloxy)-2-(trimethylsilyl)-ethanesulfonamide

There total 1 articles about (±)-N-(1-(4-chlorophenyl)but-3-enyloxy)-2-(trimethylsilyl)-ethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C10H12ClNO (936485-26-6) + 2-(trimethylsilyl)ethanesulfinic acid → (±)-N-(1-(4-chlorophenyl)but-3-enyloxy)-2-(trimethylsilyl)-ethanesulfonamide (1393744-91-6)

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;

DOI:10.1021/jo3013226

Reference yield: 62.0%

2,2,6,6-Tetramethyl-1-piperidinyloxy free radical (2564-83-2,45842-10-2,126517-51-9,25657-03-8,26933-82-4,54637-06-8,64104-42-3) + (±)-N-(1-(4-chlorophenyl)but-3-enyloxy)-2-(trimethylsilyl)-ethanesulfonamide (1393744-91-6) → (±)-1-((5-(4-chlorophenyl)-2-(2-(trimethylsilyl)-ethylsulfonyl)isoxazolidin-3-yl)methoxy)-2,2,6,6-tetramethylpiperidine

Guidance literature:

With copper(II) 2-ethylhexanoate; oxygen; potassium carbonate; In toluene; at 60 ℃; for 24h; under 760.051 Torr; stereoselective reaction; Inert atmosphere;

DOI:10.1021/jo3013226

upstream raw materials:

C₁₀H₁₂ClNO

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