2-<4-(3-hydroxy-3-methylbutyne-1-yl)phenyl>benzoxazole

Base Information

Chemical Name:2-<4-(3-hydroxy-3-methylbutyne-1-yl)phenyl>benzoxazole
CAS No.:225100-45-8
Molecular Formula:C₁₈H₁₅NO₂
Molecular Weight:277.323
Hs Code.:

Synonyms:2-<4-(3-hydroxy-3-methylbutyne-1-yl)phenyl>benzoxazole

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Chemical Property of 2-<4-(3-hydroxy-3-methylbutyne-1-yl)phenyl>benzoxazole

Chemical Property:

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Technology Process of 2-<4-(3-hydroxy-3-methylbutyne-1-yl)phenyl>benzoxazole

There total 4 articles about 2-<4-(3-hydroxy-3-methylbutyne-1-yl)phenyl>benzoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 3164-13-4
2-(4-bromophenyl)-1,3-benzoxazole

: 115-19-5
2-methyl-but-3-yn-2-ol

: 225100-45-8
2-<4-(3-hydroxy-3-methylbutyne-1-yl)phenyl>benzoxazole

Guidance literature:: With copper(l) iodide; triethylamine; triphenylphosphine; palladium dichloride; In dimethyl sulfoxide; N,N-dimethyl-formamide; for 12h; Ambient temperature;

Reference yield:

: 117649-27-1,3230-46-4
2-(4-bromo-benzylidenamino)-phenol

: 225100-45-8
2-<4-(3-hydroxy-3-methylbutyne-1-yl)phenyl>benzoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / iodosobenzene diacetate / acetonitrile / Heating

2: 58 percent / Et₃N, CuI, PdCl₂, PPh₃ / dimethylformamide; dimethylsulfoxide / 12 h / Ambient temperature

With copper(l) iodide; [bis(acetoxy)iodo]benzene; triethylamine; triphenylphosphine; palladium dichloride; In dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1122-91-4
4-bromo-benzaldehyde

: 225100-45-8
2-<4-(3-hydroxy-3-methylbutyne-1-yl)phenyl>benzoxazole

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / ethanol / Heating

2: 100 percent / iodosobenzene diacetate / acetonitrile / Heating

3: 58 percent / Et₃N, CuI, PdCl₂, PPh₃ / dimethylformamide; dimethylsulfoxide / 12 h / Ambient temperature

With copper(l) iodide; [bis(acetoxy)iodo]benzene; triethylamine; triphenylphosphine; palladium dichloride; In ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;