4-<<4-phenyl>thio>butyrate

Base Information

Chemical Name:4-<<4-phenyl>thio>butyrate
CAS No.:130198-88-8
Molecular Formula:C₁₅H₂₃NO₄S
Molecular Weight:313.418
Hs Code.:

4-<<4-<N,N-bis(2-hydroxyethyl)amino>phenyl>thio>butyrate

Synonyms:4-<<4-phenyl>thio>butyrate

Suppliers and Price of 4-<<4-phenyl>thio>butyrate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-<<4-phenyl>thio>butyrate

Chemical Property:

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Technology Process of 4-<<4-phenyl>thio>butyrate

There total 5 articles about 4-<<4-phenyl>thio>butyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 4897-84-1
Methyl 4-bromobutyrate

: 100132-31-8
4-benzenethiol

: 130198-88-8
4-<<4-phenyl>thio>butyrate

Guidance literature:: With potassium carbonate; In methanol; for 0.166667h; Heating;
DOI:10.1021/jm00173a016

Reference yield:

: 130219-46-4
S-<(benzyloxy)carbonyl>-4-aminobenzenethiol

: 130198-88-8
4-<<4-phenyl>thio>butyrate

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / AcOH / tetrahydrofuran / 336 h / 20 °C

2: 56 percent / NaOH / ethanol / 2 h / Heating

3: 56 percent / K₂CO₃ / methanol / 0.17 h / Heating

With sodium hydroxide; potassium carbonate; acetic acid; In tetrahydrofuran; methanol; ethanol;
DOI:10.1021/jm00173a016

Reference yield:

: 130198-85-5
S-<(benzyloxy)carbonyl>-4-nitrobenzenethiol

: 130198-88-8
4-<<4-phenyl>thio>butyrate

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / SnCl₂*2H₂O / ethyl acetate / 4 h / Heating

2: 79 percent / AcOH / tetrahydrofuran / 336 h / 20 °C

3: 56 percent / NaOH / ethanol / 2 h / Heating

4: 56 percent / K₂CO₃ / methanol / 0.17 h / Heating

With sodium hydroxide; potassium carbonate; acetic acid; tin(ll) chloride; In tetrahydrofuran; methanol; ethanol; ethyl acetate;
DOI:10.1021/jm00173a016