C₄₇H₆₀N₂O₁₁Si₂

Base Information

Chemical Name:C₄₇H₆₀N₂O₁₁Si₂
CAS No.:1410805-64-9
Molecular Formula:C₄₇H₆₀N₂O₁₁Si₂
Molecular Weight:885.171
Hs Code.:

C<sub>47</sub>H<sub>60</sub>N<sub>2</sub>O<sub>11</sub>Si<sub>2</sub>

Synonyms:C₄₇H₆₀N₂O₁₁Si₂

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Chemical Property of C₄₇H₆₀N₂O₁₁Si₂

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Technology Process of C₄₇H₆₀N₂O₁₁Si₂

There total 27 articles about C₄₇H₆₀N₂O₁₁Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: C₄₆H₅₆N₂O₉Si₂

: 1410805-64-9
C₄₇H₆₀N₂O₁₁Si₂

Guidance literature:: With 3C₂H₃O₂^(1-)*Ce⁽³⁺⁾*7H₂O; 2C₂H₃O₂^(1-)*Cu⁽²⁺⁾*7H₂O; oxygen; In methanol; for 44h; Inert atmosphere;
DOI:10.1021/ol302691j

Reference yield:

: C₂₈H₄₉NO₇Si₂

: 1410805-64-9
C₄₇H₆₀N₂O₁₁Si₂

Guidance literature:: Multi-step reaction with 9 steps

1: sodium periodate / tetrahydrofuran; aq. phosphate buffer / 0.2 h / 20 °C / pH 7 / Inert atmosphere

2: hydroxylamine hydrochloride; pyridine / ethanol / 2.5 h / 0 °C / Inert atmosphere

3: pyridine; N-ethyl-N,N-diisopropylamine; N-chloro-succinimide / chloroform / 44 h / 20 - 50 °C / Inert atmosphere

4: Dess-Martin periodane / dichloromethane / 3 h / 20 °C / Inert atmosphere

5: samarium diiodide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

6: Martins sulfurane / dichloromethane / 0.5 h / -78 - 20 °C / Inert atmosphere

7: CSA / methanol / 1.5 h / 0 °C / Inert atmosphere

8: methanol; Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere

9: oxygen; 3C₂H₃O₂^(1-)*Ce⁽³⁺⁾*7H₂O; 2C₂H₃O₂^(1-)*Cu⁽²⁺⁾*7H₂O / methanol / 44 h / Inert atmosphere

With pyridine; methanol; sodium periodate; N-chloro-succinimide; samarium diiodide; Martins sulfurane; 3C₂H₃O₂^(1-)*Ce⁽³⁺⁾*7H₂O; 2C₂H₃O₂^(1-)*Cu⁽²⁺⁾*7H₂O; hydroxylamine hydrochloride; oxygen; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; aq. phosphate buffer; ethanol; dichloromethane; chloroform; 5: |Reformatsky Reaction / 9: |Michael Addition;
DOI:10.1021/ol302691j

Reference yield:

: C₂₇H₄₅NO₆Si₂

: 1410805-64-9
C₄₇H₆₀N₂O₁₁Si₂

Guidance literature:: Multi-step reaction with 8 steps

1: hydroxylamine hydrochloride; pyridine / ethanol / 2.5 h / 0 °C / Inert atmosphere

2: pyridine; N-ethyl-N,N-diisopropylamine; N-chloro-succinimide / chloroform / 44 h / 20 - 50 °C / Inert atmosphere

3: Dess-Martin periodane / dichloromethane / 3 h / 20 °C / Inert atmosphere

4: samarium diiodide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

5: Martins sulfurane / dichloromethane / 0.5 h / -78 - 20 °C / Inert atmosphere

6: CSA / methanol / 1.5 h / 0 °C / Inert atmosphere

7: methanol; Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere

8: oxygen; 3C₂H₃O₂^(1-)*Ce⁽³⁺⁾*7H₂O; 2C₂H₃O₂^(1-)*Cu⁽²⁺⁾*7H₂O / methanol / 44 h / Inert atmosphere

With pyridine; methanol; N-chloro-succinimide; samarium diiodide; Martins sulfurane; 3C₂H₃O₂^(1-)*Ce⁽³⁺⁾*7H₂O; 2C₂H₃O₂^(1-)*Cu⁽²⁺⁾*7H₂O; hydroxylamine hydrochloride; oxygen; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform; 4: |Reformatsky Reaction / 8: |Michael Addition;
DOI:10.1021/ol302691j