1-(2,4,5,6-tetrafluorophenyl)-4-trimethylsilyl-2,4-diaza-1,3-dithia-2,3-butadiene

Base Information

Chemical Name:1-(2,4,5,6-tetrafluorophenyl)-4-trimethylsilyl-2,4-diaza-1,3-dithia-2,3-butadiene
CAS No.:530102-86-4
Molecular Formula:C₉H₁₀F₄N₂S₂Si
Molecular Weight:314.403
Hs Code.:

Synonyms:1-(2,4,5,6-tetrafluorophenyl)-4-trimethylsilyl-2,4-diaza-1,3-dithia-2,3-butadiene

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Chemical Property of 1-(2,4,5,6-tetrafluorophenyl)-4-trimethylsilyl-2,4-diaza-1,3-dithia-2,3-butadiene

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Technology Process of 1-(2,4,5,6-tetrafluorophenyl)-4-trimethylsilyl-2,4-diaza-1,3-dithia-2,3-butadiene

There total 3 articles about 1-(2,4,5,6-tetrafluorophenyl)-4-trimethylsilyl-2,4-diaza-1,3-dithia-2,3-butadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 503027-47-2,503027-48-3,155139-78-9,18156-25-7
N,N'-bis(trimethylsilyl)sulfurdiimide

: 530102-83-1
2,3,4,6-tetrafluorophenylsulfenyl chloride

: 530102-86-4
1-(2,4,5,6-tetrafluorophenyl)-4-trimethylsilyl-2,4-diaza-1,3-dithia-2,3-butadiene

Guidance literature:: In dichloromethane; at 20 ℃; for 16h;
DOI:10.1002/ejic.200390016

Reference yield:

: 2367-82-0
1,2,3,5-tetrafluorobenzene

: 530102-86-4
1-(2,4,5,6-tetrafluorophenyl)-4-trimethylsilyl-2,4-diaza-1,3-dithia-2,3-butadiene

Guidance literature:: Multi-step reaction with 3 steps

1.1: BuLi / hexane; diethyl ether / 1 h / -80 °C

1.2: 57 percent / sulfur / hexane; diethyl ether / -80 - 20 °C

2.1: 81 percent / Cl₂ / CCl₄ / 20 °C

3.1: 93 percent / CH₂Cl₂ / 16 h / 20 °C

With n-butyllithium; chlorine; In tetrachloromethane; diethyl ether; hexane; dichloromethane;
DOI:10.1002/ejic.200390016

Reference yield:

: 21386-20-9
2,3,4,6-tetrafluorobenzenethiol

: 530102-86-4
1-(2,4,5,6-tetrafluorophenyl)-4-trimethylsilyl-2,4-diaza-1,3-dithia-2,3-butadiene

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / Cl₂ / CCl₄ / 20 °C

2: 93 percent / CH₂Cl₂ / 16 h / 20 °C

With chlorine; In tetrachloromethane; dichloromethane;
DOI:10.1002/ejic.200390016