16-Acetylsulfanyl-hexadecanoic acid (S)-1-benzyloxymethyl-2-hexadecanoyloxy-ethyl ester

Base Information

Chemical Name:16-Acetylsulfanyl-hexadecanoic acid (S)-1-benzyloxymethyl-2-hexadecanoyloxy-ethyl ester
CAS No.:221623-65-0
Molecular Formula:C₄₄H₇₆O₆S
Molecular Weight:733.15
Hs Code.:

Synonyms:16-Acetylsulfanyl-hexadecanoic acid (S)-1-benzyloxymethyl-2-hexadecanoyloxy-ethyl ester

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Chemical Property of 16-Acetylsulfanyl-hexadecanoic acid (S)-1-benzyloxymethyl-2-hexadecanoyloxy-ethyl ester

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Technology Process of 16-Acetylsulfanyl-hexadecanoic acid (S)-1-benzyloxymethyl-2-hexadecanoyloxy-ethyl ester

There total 5 articles about 16-Acetylsulfanyl-hexadecanoic acid (S)-1-benzyloxymethyl-2-hexadecanoyloxy-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1487-50-9
1-O-hexadecanoyl-3-O-benzyl-sn-glycerol

: 139270-96-5
S-acetyl-16-mercaptohexadecanoic acid

: 221623-65-0
16-Acetylsulfanyl-hexadecanoic acid (S)-1-benzyloxymethyl-2-hexadecanoyloxy-ethyl ester

Guidance literature:: With dmap; diisopropyl-carbodiimide; In dichloromethane; at 0 - 22 ℃; for 5h;
DOI:10.1016/S0040-4039(99)00104-5

Reference yield:

: 2536-35-8
16-bromohexadecanoic acid

: 221623-65-0
16-Acetylsulfanyl-hexadecanoic acid (S)-1-benzyloxymethyl-2-hexadecanoyloxy-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / dimethylformamide / 8 h / 60 °C

2: 94 percent / diisopropylcarbodiimide, DMAP / CH₂Cl₂ / 5 h / 0 - 22 °C

With dmap; diisopropyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(99)00104-5

Reference yield:

: 506-13-8
16-hydroxyhexadecanoic acid

: 221623-65-0
16-Acetylsulfanyl-hexadecanoic acid (S)-1-benzyloxymethyl-2-hexadecanoyloxy-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / HBr / acetic acid / 72 h / Heating

2: 65 percent / dimethylformamide / 8 h / 60 °C

3: 94 percent / diisopropylcarbodiimide, DMAP / CH₂Cl₂ / 5 h / 0 - 22 °C

With dmap; hydrogen bromide; diisopropyl-carbodiimide; In dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(99)00104-5