1α-ethyl-1β-(hydroxymethyl)-1,2,3,4,6,7,12,12bβ-octahydroindolo<2,3-a>quinolizine

Base Information

• Chemical Name: 1α-ethyl-1β-(hydroxymethyl)-1,2,3,4,6,7,12,12bβ-octahydroindolo<2,3-a>quinolizine
• CAS No.: 64361-56-4
• Molecular Formula: C₁₈H₂₄N₂O
• Molecular Weight: 284.401

Synonyms:1α-ethyl-1β-(hydroxymethyl)-1,2,3,4,6,7,12,12bβ-octahydroindolo<2,3-a>quinolizine

Chemical Property of 1α-ethyl-1β-(hydroxymethyl)-1,2,3,4,6,7,12,12bβ-octahydroindolo<2,3-a>quinolizine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1α-ethyl-1β-(hydroxymethyl)-1,2,3,4,6,7,12,12bβ-octahydroindolo<2,3-a>quinolizine

There total 4 articles about 1α-ethyl-1β-(hydroxymethyl)-1,2,3,4,6,7,12,12bβ-octahydroindolo<2,3-a>quinolizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.8%

1-Benzoyloxymethyl-1-ethyl-2,3,4,6,7,12-hexahydro-1H-indolo[2,3-a]quinolizin-5-ylium; perchlorate (97720-58-6) → 1α-ethyl-1β-(hydroxymethyl)-1,2,3,4,6,7,12,12bβ-octahydroindolo<2,3-a>quinolizine (64361-56-4) + Benzoic acid (1R,12bS)-1-ethyl-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizin-1-ylmethyl ester (58451-79-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In acetone; under 760 Torr; Ambient temperature;

DOI:10.1021/jo00220a017

Reference yield:

(+)-1-acetyloxymethyl-1-ethyl-1,2,3,4,6,7,12,12b-octahydroindolo[2,3-a]quinolizine (58451-77-7,99781-90-5,106498-96-8,106498-97-9) → 14,15-dihydro-1,14-seco-21-nor-eburnamenin-20-ol (58451-76-6,64361-56-4,106498-98-0,106498-99-1,114420-88-1)

Guidance literature:

With sodium hydroxide; In methanol; water;

Reference yield:

1-ethyl-2,3,4,6,7,12-hexahydro-indolo(2,3-a)quinolizinium perchlorate (55390-29-9) → 14,15-dihydro-1,14-seco-21-nor-eburnamenin-20-ol (58451-76-6,64361-56-4,106498-98-0,106498-99-1,114420-88-1)

Guidance literature:

With sodium hydroxide; paraformaldehyde; In methanol; dichloromethane; water;

upstream raw materials:

(+)-1-acetyloxymethyl-1-ethyl-1,2,3,4,6,7,12,12b-octahydroindolo[2,3-a]quinolizine

1-ethyl-2,3,4,6,7,12-hexahydro-indolo(2,3-a)quinolizinium perchlorate

1-Benzoyloxymethyl-1-ethyl-2,3,4,6,7,12-hexahydro-1H-indolo[2,3-a]quinolizin-5-ylium; perchlorate

Downstream raw materials:

1-(3,4,5-Trimethoxybenzoyloxymethyl)-1-ethyl-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizine

Benzoic acid (1S,12bS)-1-ethyl-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizin-1-ylmethyl ester

(+/-)-apovincamine

ethyl eburnamenine-14-carboxylate

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 64361-56-4 1α-ethyl-1β-(hydroxymethyl)-1,2,3,4,6,7,12,12bβ-octahydroindolo<2,3-a>quinolizine

Send

Send

Metric Ton KG G Pound L ML

Send

Send